Stabilized pre-fusion rsv f proteins
A pre-fusion, protein technology, applied in the medical field, can solve the problem of no vaccine and so on
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[0127] Example 1 : Stability of prefusion conformations of RSV F variants in culture supernatants
[0128] The RSV F sequence used as a control for stability studies was based on the consensus sequence of the A subtype (SEQ ID NO: 13) or the consensus sequence of the B subtype (SEQ ID NO: 14), because the consensus sequence will correspond to the clinical isolate. The wild-type (non-passage) sequences of the strains are very similar (Kumaria et al. (2011)). For detection purposes, the F protein was fused at the C-terminus to a strep-tag. To assess the stability of various point mutations in RSV F, the amount of F protein in the prefusion conformation was measured in AlphaLISA.
[0129] By adding 5 μl of RSV F sample to 25 μl of prefusion specific Mab CR9501 (0.8 nM), anti-human IgG acceptor beads and streptavidin donor beads (Perkin Elmer) in The assay was performed in the mixture in assay buffer. After incubating the mixture for 2.5 hours at room temperature, the chemilu...
example 2
[0130] Example 2: Stable prefusion RSV F polypeptide - preparation of stabilizing mutations
[0131] Soluble prefusion proteins based on consensus RSV F (SEQ ID NO: 13 or 14) could not be purified due to apparent instability (e.g. image 3 , 4 shown). for evaluation image 3 Some of the stabilizing mutations shown in , in addition to the previously described D486N stabilizing mutation (Krarup et al., 2015), also produced two mutations containing a stable prefusion conformation, notably mutations P101Q and I152V in RSV-F protein (RSV180305; SEQ ID NO:20). In addition, another stable prefusion F protein (RSV172527; SEQ ID NO:21) was generated in which the P101Q and I152V substitutions were introduced in the prefusion RSV F protein, which already contained several previously described Stabilizing substitutions, in particular the mutations S46G, L203I, S215P, T357R, N371Y, D486N and D489Y. These constructs were synthesized and codon optimized at Gene Technologies, Inc. (Lif...
example 3
[0133] Example 3: SDS-PAGE analysis.
[0134] Purified RSV172527 was analyzed on 4%-12% (w / v) Bis-Tris NuPAGE gels, 1x MOPS (Life Technologies) under reducing or non-reducing conditions. All procedures were performed according to the manufacturer's instructions. For purity analysis, the gel was stained with Krypton Infrared protein stain (Thermo Scientific). Non-reduced and reduced RSV172527 were pure and in F 0 and F 1 Bands are separately visible at the expected height of the extracellular domain.
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