Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Process and system for increasing the solids content of microfibrillated cellulose

A solid content, cellulose technology, applied in the direction of drying solid materials without heating, post-treatment modification of cellulose pulp, drying solid materials, etc., can solve problems such as unsatisfactory results

Pending Publication Date: 2021-07-23
宝丽格公司
View PDF7 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, it is often challenging to remove solvent / water from products with high solvent / water retention
The inventors have found that satisfactory results cannot be obtained for solvent removal from suspensions comprising microfibrillated cellulose using conventional filtration methods, in particular press filtration as known in the art

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Process and system for increasing the solids content of microfibrillated cellulose
  • Process and system for increasing the solids content of microfibrillated cellulose
  • Process and system for increasing the solids content of microfibrillated cellulose

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0126] Preparation of microfibrillated cellulose

[0127] MFC is commercially available and commercialized as "Exilva" based on cellulose pulp from Norway spruce (softwood). The starting solids content of the microfibrillated cellulose used for solvent removal was 2%.

[0128] MFC is available in two different qualities called Microfibrillated Cellulose P and Microfibrillated Cellulose F. The difference between microfibrillated cellulose P and microfibrillated cellulose F is mainly related to the size of the microfibril aggregates and thus to the 3D network properties. Microfibrillated cellulose "F" has higher Brookfield viscosity, surface area (water retention) and higher tensile strength than microfibrillated cellulose "P". Although these differences are not relevant to the working of the present invention, the removal of solvent from these two different microfibrillated cellulose materials shows that the method according to the present invention is applicable to differe...

Embodiment 2

[0130] Solvent removal (dehydration) of 2% MFC "F" in a laboratory scale system according to the invention

[0131] 2% MFC "F" was conditioned overnight in a heating cabinet.

[0132] Figure 5 It is shown how the choice of porous substrate (tape) and temperature affects the filtration capacity.

[0133] In a specific example, the following porous substrates were tested: Valmet S5111-L1, Valmet S2121-L2K2, Safar Tetex DLW 07-8435-SK010, Maro S35, Maro S25.

[0134] Vacuum set to 450mbar

[0135] Filtration time 220 seconds

[0136] Filter cake thickness: 6-7mm (about 70g)

[0137] Dry content measured after drying the filter cake in a heating cabinet at 105°C

[0138] Visual observation of the filtrate and calculation of yield from dry content measurements showed no discernible loss of fibrils through the substrate.

Embodiment 3

[0140] The Effect of pH Value on Filtration Capacity

[0141] Figure 6 Shows how choice of pH affects filterability

[0142] Solvent removal (dehydration) of 2% MFC "F" performed in a laboratory scale setup.

[0143] 2% MFC "F" was conditioned overnight in a heating cabinet.

[0144] Vacuum set to 450mbar

[0145] Porous substrates tested: Valmet S4152-l2K2 and Valmet S4152-L2K2-M7

[0146] Filter time 180 and 220 seconds

[0147] Filter cake 6-7mm (about 70g)

[0148] Dry content measured after drying the filter cake in a heating cabinet at 105°C

[0149] Visual observation of the filtrate and calculation of yield from dry content measurements showed no discernible loss of fibrils through the substrate.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The present invention relates to a process and a system for the at least partial removal or exchange of solvent from / in a suspension comprising microfibrillated cellulose (MFC), specifically the at least partial removal of solvent from a suspension comprising microfibrillated cellulose having a comparatively high solvent (water) content to a relatively lower solvent content. Accordingly, the solids content of the microfibrillated cellulose increases during the the step of at least partial removal of solvent from a suspension comprising process, in particular from a first solids content in the range of from 0.1 % weight by weight ("w / w") to 6 % w / w, preferably 1 % weight by weight ("w / w") to 5% w / w, up to a second solids content of above 5 % w / w, preferably to a solids content of from above 5 % w / w - 50% w / w, further preferably to a solids content of from above 5 % w / w - 25% w / w. In a separate aspect, a solvent exchange step after the at least partial removal of a first solvent is also part of the present invention.

Description

technical field [0001] The present invention relates to a process for the at least partial removal of solvent, in particular water, from a suspension comprising microfibrillated cellulose (MFC), in particular water, wherein the suspension The liquid changes from a relatively high solvent content, especially water content, to a relatively low solvent content. Thus, during said at least partial solvent removal, the solids content of the microfibrillated cellulose is increased, in particular from 0.1% weight / weight ("w / w") to 6% w / w, preferably 1% w Microfibrillated fibers having a first solids content of microfibrillated cellulose increased to 5% w / w or more in the range of / w to 5% w / w, more preferably 1.5% w / w to 3.5% w / w A second solids content of cellulose, preferably 5% w / w to 50% w / w solids of microfibrillated cellulose, more preferably 6% w / w to 30% w / w solids of microfibrillated cellulose content, more preferably 7% w / w - 20% w / w solids content of the fibrillated cellu...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): F26B17/02F26B5/12C09D101/00D21H11/18
CPCF26B5/12F26B17/023D21H11/18C08L1/02C08B1/003D21H11/08D21C9/18
Inventor 汉斯·亨里克·奥夫雷博赛德·阿里·莫萨维·法尔
Owner 宝丽格公司
Features
  • Generate Ideas
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More