Compound, photocurable composition, cured film, and organic EL element
A photocurable and photocurable resin technology, applied in the fields of cured films, organic EL elements, photocurable compositions, and compounds, which can solve the problems of inability to coat the composition, increased viscosity, and short usable time.
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[0080] Hereinafter, the present invention will be described more specifically with reference to examples. However, the present invention is not limited to these Examples.
[0081] [Synthesis of Compound (Water Capture Component)] (Example 1)
[0082] Put trimethylolpropane diallyl ether (2,2-bis(allyloxymethyl)-1-butanol, a compound represented by formula (3-1)) into the flask (trade name: new Allyl T-20, 21 parts by mass of OSAKA SODA CO., LTD.) and 10 parts by mass of tetrapropoxy zirconium (Tokyo Chemical Industry Co., Ltd.) were stirred at 25° C. for 1 hour. Then, the volatile components were distilled off under reduced pressure at 60° C. and 300 Pa for 3 hours, and the volatile components were further distilled under reduced pressure at 150° C. and 300 Pa for 3 hours to obtain the compound of Example 1 as a transparent viscous body. Since 4 equivalents of trimethylolpropane diallyl ether were reacted with tetrapropoxyzirconium, it is speculated that the compound of Exam...
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