The invention provides a method for enriching
zirconium,
lithium and
titanium elements from
coal gangue and / or
fly ash, which comprises the following steps: S1, taking
coal gangue and / or
fly ash, adding a gelatinizing agent, mixing,
roasting, washing with water, and adding
dilute acid to prepare gel I; s2, adding a treating agent into
coal gangue and / or
fly ash,
roasting, and adding water for washing to form
slurry I; s3, adding the
slurry I into the gel I, stirring, reacting, layering and separating to obtain gel II and
slurry II; s4, the gel II is subjected to acid
pickling with an acid
pickling solution and separated, and filtrate containing
zirconium,
lithium and
titanium elements and gel III are obtained; and S5, extracting the filtrate by using an
organic solvent, and carrying out back extraction on an organic phase by using an acid solution to obtain a solution containing
zirconium,
lithium,
titanium and other element atoms, thereby realizing enrichment of zirconium, lithium and titanium elements. In the technological process, all raw materials and reagents can be recycled,
pollution is avoided, the cost is low, and the separation
recovery rate is high.