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46results about How to "Change surface state" patented technology

Chemical granulation processing method for quartz surface

A method for chemically and roughly treating a quartz surface overcomes the defects of the prior art in which the treatment to the quartz surface easily leads to damage and influences the size accuracy of the quartz product. The method is as below: at a normal temperature and a normal pressure, immersing a quartz product into a container filled with a treating fluid so as to undergo reaction after the surface of the quartz product is polished, taking out the quartz product after two-hour reaction, and immersing the quartz product into the treating fluid again so as to repeat the preceding reaction till the roughness Ra of the surface of the quartz product is equal to 1.5 micrometers to 4.5 micrometers after attachments on the surface of the quartz product is eliminated with deionized water. The treatment process has reasonable design, involves simple devices and is easy to be operated, and the obtained quartz product has uniform surface roughness which is free from the influence of the shape. During the participation in the CVD reaction, the crazing and the shedding of a deposited film on the quartz surface is effectively reduced so as to reduce the possibility of pollution to the reaction cavity, to remarkably improve the finished product rate and the production efficiency, and then further to prolong the service life of the quartz product, save time, reduce consumption and reduce production cost.
Owner:SHENYANG HANKE SEMICON MATERIALS

Method for preparing cobalt-doped zinc oxide nanorods through sol-gel

The invention discloses a method for preparing cobalt-doped zinc oxide nanorods through sol-gel. The method comprises the steps of dissolving dihydrate zinc acetate and tetrahydrate cobaltous acetate into ethylene glycol monomethyl ether according to the stoichiometric ratio of Zn<1-x>Co<x>O, stirring the mixture uniformly, and obtaining a mixed solution; dropwise adding ethanolamine to the mixed solution, conducting a reaction under the condition that the mixture is stirred at the temperature of 60-80 DEG C, cooling the mixture naturally to the room temperature after the reaction is ended, and obtaining clear cobalt-doped zinc oxide precursor sol; drying the clear cobalt-doped zinc oxide precursor sol, obtaining dried gel, then making the dried gel be subjected to a heat treatment process in the air atmosphere, and obtaining the clear cobalt-doped zinc oxide nanorods. According to the method, the cobalt-doped zinc oxide nanorods are prepared through a multicomponent uniform reaction sol-gel method, and the method has the advantages that the process is simple, the reaction temperature is low, the cost is low, the test process is easy to control, the product crystallinity degree is high, and the crystalline phase is pure, and the obtained clear cobalt-doped zinc oxide nanorods have ferromagnetism at the room temperature.
Owner:XIAN TECHNOLOGICAL UNIV

Compound coated slow-release fertilizer for garden planting and method for preparing compound coated slow-release fertilizer

The invention discloses a compound coated slow-release fertilizer for garden planting. The compound coated slow-release fertilizer comprises kernel fertilizers, inner-layer coating materials and outer-layer coating materials. The inner-layer coating materials wrap the surfaces of the kernel fertilizers, and the outer-layer coating materials wrap the surfaces of the inner-layer coating materials; urea, diammonium phosphate, potassium sulfate and grass carbon are mixed with one another to obtain the kernel fertilizers; a process for preparing the inner-layer coating materials include uniformly mixing corn starch and water with each other to obtain first mixtures, adding hydrogen peroxide and sodium hydroxide solution A into the first mixtures to obtain second mixtures, heating the second mixtures, then preserving heat of the second mixtures, adding sodium bisulfite solution into the second mixtures to obtain third mixtures, cooling the third mixtures, adding epichlorohydrin into the third mixtures to obtain fourth mixtures, dropwise adding sodium hydroxide solution B into the fourth mixtures to obtain fifth mixtures, carrying out constant-temperature reaction on the fifth mixtures and cooling reaction products until the temperatures of the reaction products reach the room temperature to obtain the inner-layer coating materials. The invention further discloses a method for preparing the compound coated slow-release fertilizer for garden planting. The compound coated slow-release fertilizer and the method have the advantages that the slow-release fertilizer prepared by the aid of the method is excellent in fertilizer efficiency slow-release and waterproof property, free of biological toxicity, good in film-forming ability and high in cohesiveness, and growth of garden crops can be promoted.
Owner:天长市天兴园林绿化工程有限公司

Antistatic plastic composite material for electric power fitting and preparation method of antistatic plastic composite material

The invention discloses an antistatic plastic composite material for an electric power fitting. The antistatic plastic composite material is prepared from the following raw materials in parts by weight: 100 parts of junked and abandoned nylon 66 plastic, 2.5 to 2.8 parts of polybutadiene epoxy resin, 23 to 27 parts of glass fiber, 9 to 10 parts of aluminum nitride, 1.7 to 1.9 parts of nano calcium carbonate, 6 to 8 parts of dimethyl formamide, 2.6 to 2.9 parts of triethylene glycol diisooctoate, 7 to 9 parts of silane coupling agent KH560, 11 to 13 parts of sericite powder, 1.4 to 1.7 parts of secondary-alkyl sulfonate and 4 to 6 parts of polyethylene wax. Nylon is modified into a matrix through the epoxy resin; the modified glass fiber is used as a reinforcing material; the nano calcium carbonate is added into the material after being subjected to graft modification treatment through the dimethyl formamide; afterwards, the composite material prepared by matching with other effective components is used for better solving the problems of magnetic hysteresis loss and eddy current loss, avoids electric energy loss, and has the advantages of being antistatic, resistant to wear and high in mechanical strength, and the like.
Owner:马鞍山市华能电力线路器材有限责任公司

Etching device for fine circuit

The invention relates to an etching device for a fine circuit and belongs to the technical field of circuit board manufacturing. The etching device comprises an etching spraying disc and a bearing plate, wherein the bearing plate bears a product below the product, the etching spraying disc is arranged above the product, the etching spraying disc is composed of multiple rows of etching nozzles, thenozzles of the etching spraying disc continuously spray etching liquid to the product below at a certain pressure for etching, and a baffle is arranged above the front end of the product in the advancing direction; the baffle plate is arranged at the front end of the etching spray disc, the bottom of the baffle plate is provided with a spoiler, the baffle plate prevents spray liquid medicine fromsplashing to a pretreatment surface of a product, and the spoiler prevents the liquid medicine from flowing back to the pretreatment surface of the product. The etching device is advantaged in that the etching liquid can be effectively prevented from being contacted with the pretreatment surface of the product too early due to sputtering and backflow, and a surface state of the product is changed, so etching precision of a circuit is ensured; the influence of the pool effect on the line precision can be effectively reduced or reduced, and the waste of the etching liquid and the pollution to the liquid medicine of the next treatment tank are avoided.
Owner:LEADER TECH ELECTRONICS SHENZHEN INC

Preparation method of electrolytic solution and black coating for micro-arc oxidation of magnesium alloy surface

The invention discloses a preparation method of an electrolytic solution for micro-arc oxidation on the surface of a magnesium alloy and a black coating. The electrolytic solution includes a main film-forming agent, an auxiliary film-forming agent, a main coloring salt, a complexing agent and deionized water; the main coloring salt is metal copper salt; the complexing agent is composed of polycondensed phosphate, organic phosphonate and tartrate; and in the electrolyte solution, the content of the main film-forming agent is 5~50 g / L; the content of the auxiliary film-forming agent is 1~ 30 g / L; the content of the main coloring salt is 1~20 g / L; the content of various complexing agents can be compounded at 1~20 g / L. The electrolyte solution is not easy to produce precipitation in the micro-arc oxidation process, has high stability, and has a long service life; the electrical parameters can also be adjusted in a wide range, and extreme discharge is not easy to occur, and the film forming efficiency is high; and the electrolyte solution is used The prepared black coating has high blackness, slight color difference, low surface roughness, high hardness, good corrosion resistance, strong adhesion, is not easy to decolorize, and has excellent thermal control performance.
Owner:SICHUAN UNIVERSITY OF SCIENCE AND ENGINEERING

Production method of multilayer printed circuit board

The invention discloses a production method of a multilayer printed circuit board. The method specifically comprises the steps of S1, preparing an inner-layer board; S2, carrying out surface treatmenton the inner-layer board; S3, preparing a prepreg; S4, superposing the inner-layer board and the prepreg through a laminating machine, and then laminating the inner-layer board and the prepreg; S5, conducting drilling and copper deposition, enabling the laminated circuit board to be sequentially subjected to the procedures of drilling, deburring, photoresist residue removal, chemical copper deposition and electroplating, and communicating the upper inner-layer board and the lower inner-layer board; S6, preparing an outer-layer board; S7, carrying out wet ink character printing by adopting full-automatic equipment; and S8, carrying out size, surface defect and electrical property detection on the printed circuit board product, and packaging the qualified product. According to the invention, the inner-layer board is produced by a subtracting method, the outer-layer board is produced by an addition method, the two methods are combined, the production efficiency can be greatly improved, and by improving and optimizing the reagent formula of the prepreg and the surface structure of the inner-layer board, the physical performance of the prepreg is improved, the strength of the multilayer circuit board is improved, and looseness is avoided.
Owner:SHENZHEN TONGCHUANGXIN ELECTRONICS

Chemical granulation processing method for quartz surface

A method for chemically and roughly treating a quartz surface overcomes the defects of the prior art in which the treatment to the quartz surface easily leads to damage and influences the size accuracy of the quartz product. The method is as below: at a normal temperature and a normal pressure, immersing a quartz product into a container filled with a treating fluid so as to undergo reaction after the surface of the quartz product is polished, taking out the quartz product after two-hour reaction, and immersing the quartz product into the treating fluid again so as to repeat the preceding reaction till the roughness Ra of the surface of the quartz product is equal to 1.5 micrometers to 4.5 micrometers after attachments on the surface of the quartz product is eliminated with deionized water. The treatment process has reasonable design, involves simple devices and is easy to be operated, and the obtained quartz product has uniform surface roughness which is free from the influence of the shape. During the participation in the CVD reaction, the crazing and the shedding of a deposited film on the quartz surface is effectively reduced so as to reduce the possibility of pollution to thereaction cavity, to remarkably improve the finished product rate and the production efficiency, and then further to prolong the service life of the quartz product, save time, reduce consumption and reduce production cost.
Owner:SHENYANG HANKE SEMICON MATERIALS

Preparation method of composite film layer on surface of rare earth magnesium alloy structural part

ActiveCN112251790AMeet assembly dimensional tolerance requirementsReduce electrophoresis voltageAnodisationElectrophoretic coatingsElectrolytic agentMicro arc oxidation
The invention discloses a preparation method of a composite film layer on the surface of a rare earth magnesium alloy structural part. The preparation method sequentially comprises the steps of oil removal, primary water washing, micro-arc oxidation, secondary water washing, electrophoresis, tertiary water washing and drying and curing. A micro-arc oxidation electrolyte is an aqueous solution containing sodium silicate, sodium fluoride, sodium hydroxide, graphene, Cu(NO3)2 and triethanolamine, electrical parameters of micro-arc oxidation are as follows: the positive current density is 5-15A/dm<2>, the negative current density is 2-3A/dm<2>, the positive duty ratio is 25-70%, the negative duty ratio is 40-50%, the positive frequency is 200-800Hz, the negative frequency is 300-500Hz, the positive and negative stages are both one stage, the micro-arc oxidation time is 10-20 min, electrophoresis liquid for electrophoresis is an aqueous solution containing acrylate, a delustering agent andcarbon black pigment, and electrical parameters of electrophoresis are as follows: the voltage is 50-80V, and the time is 10-30s; and through the coordination effect of micro-arc oxidation and electrophoresis, the composite film layer meeting the requirements of high hardness, high bonding strength and ultraviolet aging resistance at the same time can be prepared.
Owner:725TH RES INST OF CHINA SHIPBUILDING INDAL CORP

Magnetic powder activation method for magnetic asphalt, magnetic asphalt preparation method, asphalt plate pouring method and waterproof bonding layer paving method

The invention discloses a magnetic powder activation method for magnetic asphalt, a magnetic asphalt preparation method, an asphalt plate pouring method and a waterproof bonding layer paving method. Firstly, an ultrasonic device is adopted to achieve effective modification of a silane coupling agent in a base solution on the surface of magnetic powder so as to reduce agglomeration of magnetic powder particles in the preparation process of the magnetic asphalt, the magnetic powder with good dispersity is obtained, then the magnetic powder and the asphalt are mixed at different shearing rates and shearing time, the prepared magnetic asphalt is magnetized, and finally, fibers are embedded into a template for pouring, and the magnetic fiber asphalt plate capable of being used for paving the waterproof bonding layer of the steel bridge deck is prepared. The magnetic powder in the prepared magnetic asphalt is uniform in dispersion and free of agglomeration, the magnetic asphalt has high residual magnetism and coercive force, the bonding effect and deformation compliance between a waterproof bonding layer and a steel plate can be improved, the tensile strength of the magnetic asphalt can be improved through embedding of fibers, the service life is prolonged, and the magnetic fiber asphalt plate is simple in preparation method and low in transportation cost, and the pavement process is simple and convenient, and the method has important construction popularization significance.
Owner:GUANGXI TRANSPORTATION SCI & TECH GRP CO LTD +2

A kind of high temperature and high humidity resistant fluoride red phosphor and preparation method thereof

The invention provides a high-temperature-resistant and high-humidity-resistant fluoride red fluorescent powder and a preparation method thereof. The fluorescent powder has a general chemical formula of KmAnM1-xF6: xMn<4+>. In the general chemical formula, A is one or two selected from the group consisting of Cu, Ba and Zn; M is at least one selected from the group consisting of Ti, Si and Ge; m + 2n are equal to 2; n is no less than 0.05 and no more than 0.2; m is no less than 1.6 and no more than 1.9; x is more than 0 and less than 0.2; and the surface of the fluorescent powder is coated with a mixture of potassium silicate, carboxymethyl cellulose sodium and polyethylene glycol. The fluorescent powder provided by the invention can be effectively excited by light with the excitation wavelength being in a range of 300 to 500 nm, so red light with a peak wavelength of 610 to 650 nm and a half-peak breadth of only 2 to 9 nm is generated, and high color purity is obtained. The preparation method provided by the invention has simple flow, can prepare target products at low temperature and under normal pressure, and facilitates to large-scale industrial production; and a special coating technology is adopted in the invention, and a coating reagent is utilized to change the surface state of fluorescent powder particles, so the problem of agglomeration of solid particles can be effectively solved, and a fluorescent powder product with good dispersion properties and high-temperature-resistant and high-humidity-resistant performances can be obtained.
Owner:HEBEI LIFU CHEM TECH

A sol-gel preparation method of cobalt-doped zinc oxide nanorods

The invention discloses a method for preparing cobalt-doped zinc oxide nanorods through sol-gel. The method comprises the steps of dissolving dihydrate zinc acetate and tetrahydrate cobaltous acetate into ethylene glycol monomethyl ether according to the stoichiometric ratio of Zn<1-x>Co<x>O, stirring the mixture uniformly, and obtaining a mixed solution; dropwise adding ethanolamine to the mixed solution, conducting a reaction under the condition that the mixture is stirred at the temperature of 60-80 DEG C, cooling the mixture naturally to the room temperature after the reaction is ended, and obtaining clear cobalt-doped zinc oxide precursor sol; drying the clear cobalt-doped zinc oxide precursor sol, obtaining dried gel, then making the dried gel be subjected to a heat treatment process in the air atmosphere, and obtaining the clear cobalt-doped zinc oxide nanorods. According to the method, the cobalt-doped zinc oxide nanorods are prepared through a multicomponent uniform reaction sol-gel method, and the method has the advantages that the process is simple, the reaction temperature is low, the cost is low, the test process is easy to control, the product crystallinity degree is high, and the crystalline phase is pure, and the obtained clear cobalt-doped zinc oxide nanorods have ferromagnetism at the room temperature.
Owner:XIAN TECH UNIV
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