The invention belongs to the technical field of
wastewater treatment, and particularly relates to an acidic surface treatment
wastewater resource utilization method which comprises the following steps: S1, adding an
oxidizing agent into acidic surface treatment
wastewater to carry out oxidation-reduction reaction to obtain a pretreatment solution; s2, mixed alkali is added into the pretreatment liquid, the pH of the pretreatment liquid is adjusted to 1.0-2.5, stirring and filter pressing are conducted, and
copper-
nickel-containing filtrate and
calcium phosphate are obtained; s3, continuously adding mixed alkali into the
copper-
nickel-containing filtrate, adjusting the pH value of the
copper-
nickel-containing filtrate to 2.5-3.0, stirring, and carrying out filter pressing to obtain nickel-containing filtrate and copper
sludge; s4, continuously adding mixed alkali into the nickel-containing filtrate, adjusting the pH value of the nickel-containing filtrate to 6.5-7.0, and carrying out filter pressing to obtain a
calcium ammonium nitrate evaporation stock solution and nickel mud; and S5, evaporating, concentrating, crystallizing and granulating the
calcium ammonium nitrate evaporation stock solution to obtain
calcium ammonium nitrate. By means of the method,
calcium ammonium nitrate can be prepared, the copper
recovery rate can reach 99.7% or above, and the nickel
recovery rate can reach 99.1% or above.