A kind of high thermal conductivity photocurable coating for optical fiber, and its preparation and application
A light-curing coating and high thermal conductivity technology, applied in the direction of optical waveguide light guide, cladding optical fiber, polyester coating, etc., can solve the problems of low thermal conductivity of optical fiber coating, low thermal conductivity of coating, low thermal expansion coefficient, etc., to achieve Enhanced interfacial compatibility, good gloss, and low thermal expansion coefficient
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Embodiment 1
[0035] The photocurable coating with high thermal conductivity for optical fiber in this embodiment includes acrylate resin, inorganic thermal conductive particles modified by vinyl silane coupling agent, reactive diluent, and photoinitiator. The acrylate resin is bisphenol A epoxy acrylate resin; the inorganic heat-conducting particles modified by the vinyl silane coupling agent are nano-Al particles modified by vinyl triethoxysilane 2 o 3 ; The reactive diluent is glycidyl methacrylate, and the addition ratio is 20wt% of bisphenol A epoxy acrylate resin; the photoinitiator is (2,4,6-trimethylbenzoyl) diphenyl Phosphine oxide, the addition ratio is 3wt% of bisphenol A epoxy acrylate resin.
[0036] The preparation method of the high thermal conductivity photocurable coating for the optical fiber comprises the following steps:
[0037] (1) Using vinyltriethoxysilane to nano-Al 2 o 3 treated to prepare vinyltriethoxysilane-modified nano-Al 2 o 3 :
[0038] In a 500mL rou...
Embodiment 2
[0045] The photocurable coating with high thermal conductivity for optical fiber in this embodiment includes acrylate resin, inorganic thermal conductive particles modified by vinyl silane coupling agent, reactive diluent, and photoinitiator. The acrylate resin is bisphenol A epoxy acrylate resin; the inorganic heat-conducting particles modified by the vinyl silane coupling agent are nano AlN modified by γ-methacryloxypropyltrimethoxysilane (i.e. aluminum nitride); the reactive diluent is tripropylene glycol diacrylate, and the addition ratio is 20wt% of bisphenol A epoxy acrylate resin; the photoinitiator is 2,4,6-trimethyl Benzoyl phenyl phosphonic acid ethyl ester, the addition ratio is 3wt% of bisphenol A epoxy acrylate resin.
[0046] The preparation method of the high thermal conductivity photocurable coating for the optical fiber comprises the following steps:
[0047] (1) Nano-AlN was treated with γ-methacryloxypropyltrimethoxysilane to prepare γ-methacryloxypropyltri...
Embodiment 3
[0055] The photocurable coating with high thermal conductivity for optical fiber in this embodiment includes acrylate resin, inorganic thermal conductive particles modified by vinyl silane coupling agent, reactive diluent, and photoinitiator. The acrylate resin is bisphenol A epoxy acrylate resin; the inorganic heat-conducting particles modified by the vinyl silane coupling agent are nano-Al particles modified by vinyl triethoxysilane 2 o 3 ; The reactive diluent is glycidyl methacrylate, and the addition ratio is 20wt% of bisphenol A epoxy acrylate resin; the photoinitiator is (2,4,6-trimethylbenzoyl) diphenyl Phosphine oxide, the addition ratio is 3wt% of bisphenol A epoxy acrylate resin.
[0056] The preparation method of the high thermal conductivity photocurable coating for the optical fiber comprises the following steps:
[0057] (1) Using vinyltriethoxysilane to nano-Al 2 o 3 treated to prepare vinyltriethoxysilane-modified nano-Al2 o 3 :
[0058] In a 500mL round...
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