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48results about How to "Inhibition of hydrolysis" patented technology

Preparation method of magnesium-rare earth alloy electrolysis raw material

The invention discloses a preparation method of magnesium-rare earth alloy electrolysis raw material. The preparation method comprises the following steps: S1, bischofite and first hydrated rare-earthchloride are mixed, and then dehydrated raw material is obtained; S2, first-stage fluidization dehydration is carried out on the dehydrated raw material at the temperature of 170-180 DEG C, and thena first-stage dehydrated crude product is obtained; S3, second-stage fluidization dehydration is carried out on the first-stage dehydrated crude product at the temperature of 230-250 DEG C, and then asecond-stage dehydrated crude product is obtained; and S4, third-stage fluidization dehydration is carried out on the second-stage dehydrated crude product at the temperature of 260-280 DEG C and inthe hydrogen chloride gas atmosphere, so that the magnesium-rare earth alloy electrolysis raw material is obtained. According to the preparation method of the magnesium-rare earth alloy electrolysis raw material, staged fluidization dehydration on the bischofite and the hydrated rare-earth chloride is carried out, the hydrogen chloride protective gas atmosphere is provided, so that a hydrolysis effect is effectively inhibited in the process that an intermediate product is dehydrated to form the magnesium-rare earth alloy electrolysis raw material, and product purity is greatly improved; and the preparation method is low in dehydration temperature, low in preparation cost and good in dehydration effect.
Owner:QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI

Preparation method of anhydrous lanthanum chloride

The invention discloses a preparation method of anhydrous lanthanum chloride. The preparation method comprises the following steps: S1, carrying out first-section fluidization dehydration on lanthanum chloride heptahydrate at 60 DEG C to 100 DEG C to obtain a lanthanum chloride trihydrate crude product; S2, carrying out second-section fluidization dehydration on the lanthanum chloride trihydrate crude product at 120 DEG C to 130 DEG C to obtain a lanthanum chloride monohydrate crude product; S3, carrying out third-section fluidization dehydration on the lanthanum chloride monohydrate crude product at 140 DEG C to 160 DEG C to obtain the anhydrous lanthanum chloride, wherein the three sections of fluidization dehydration are carried out in a hydrogen chloride gas atmosphere. According to the preparation method of the anhydrous lanthanum chloride, disclosed by the invention, the lanthanum chloride heptahydrate is subjected to sectioned fluidization dehydration and a hydrogen chloride protection gas atmosphere is provided, so that a hydrolysis effect in a process of dehydrating an intermediate product lanthanum chloride monohydrate into the anhydrous lanthanum chloride is effectively inhibited and the purity of a product is greatly improved; the preparation method of the anhydrous lanthanum chloride has the advantages of low dehydration temperature, low preparation cost and good dehydration effect.
Owner:QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI

Preparation method for anhydrous rare earth chloride

The invention discloses a preparation method for an anhydrous rare earth chloride. The method comprises the following steps: step 1, performing first-stage fluidization dehydration on a rare earth chloride heptahydrate under the temperature of 60 DEG C-100 DEG C to obtain a crude product of a rare earth chloride trihydrate; step 2, performing second-stage fluidization dehydration on the crude product of the rare earth chloride trihydrate under the temperature of 120 DEG C-130 DEG C to obtain a crude product of a rare earth chloride monohydrate; and step 3, performing third-stage fluidization dehydration on the crude product of the rare earth chloride monohydrate under the temperature of 140 DEG C-160 DEG C to obtain the anhydrous rare earth chloride, wherein the third-stage fluidization dehydration is carried out in a hydrogen chloride gas atmosphere. According to the preparation method for the anhydrous rare earth chloride provided by the invention, the rare earth chloride heptahydrate is subjected to staged fluidization dehydration, and the hydrogen chloride protection gas atmosphere is provided, so that hydrolysis in the process of dehydration of the intermediate product rare earth chloride monohydrate to the anhydrous rare earth chloride is effectively inhibited, and the product purity is greatly improved; and the preparation method for the anhydrous rare earth chloride hasthe advantages of a low dehydration temperature, low preparation costs and good dehydration effects.
Owner:QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI

Antistatic plastic composite material for electric power fitting and preparation method of antistatic plastic composite material

The invention discloses an antistatic plastic composite material for an electric power fitting. The antistatic plastic composite material is prepared from the following raw materials in parts by weight: 100 parts of junked and abandoned nylon 66 plastic, 2.5 to 2.8 parts of polybutadiene epoxy resin, 23 to 27 parts of glass fiber, 9 to 10 parts of aluminum nitride, 1.7 to 1.9 parts of nano calcium carbonate, 6 to 8 parts of dimethyl formamide, 2.6 to 2.9 parts of triethylene glycol diisooctoate, 7 to 9 parts of silane coupling agent KH560, 11 to 13 parts of sericite powder, 1.4 to 1.7 parts of secondary-alkyl sulfonate and 4 to 6 parts of polyethylene wax. Nylon is modified into a matrix through the epoxy resin; the modified glass fiber is used as a reinforcing material; the nano calcium carbonate is added into the material after being subjected to graft modification treatment through the dimethyl formamide; afterwards, the composite material prepared by matching with other effective components is used for better solving the problems of magnetic hysteresis loss and eddy current loss, avoids electric energy loss, and has the advantages of being antistatic, resistant to wear and high in mechanical strength, and the like.
Owner:马鞍山市华能电力线路器材有限责任公司

Method for preparing high-strength brick by synergistically utilizing waste incineration fly ash and steel slag

The invention discloses a method for preparing a high-strength brick by synergistically utilizing waste incineration fly ash and steel slag, the method comprises the following steps: (1) grinding the steel slag to obtain steel slag powder; (2) grinding blast furnace slag to obtain blast furnace slag powder; (3) mixing the steel slag powder, the blast furnace slag powder and the fly ash to obtain fly ash mixed powder; (4) mixing water and the fly ash mutual doping powder, uniformly stirring, putting into a mold, and curing to obtain an anode assembly block; (5) mixing sodium phosphate and sodium silicate to obtain a silicon phosphorus reagent; (6) mixing a silicon-phosphorus reagent with water, and stirring until sodium phosphate and sodium silicate are completely dissolved to obtain a silicon-phosphorus solution; (7) adding ethanol into the silicon-phosphorus solution to obtain an electrolyte; and (8) connecting the anode assembly block to an anode, soaking the anode assembly block in the electrolyte, connecting a direct-current power supply, activating, taking down the anode assembly block, and maintaining to obtain the high-strength brick. The process is simple, and the waste incineration fly ash can be converted into the high-strength bricks through operation in a normal-temperature environment.
Owner:浙江中陶环保科技集团有限公司

Multifunctional polymer and preparation method and application thereof

The invention relates to a high molecular compound, in particular to a multifunctional polymer and a preparation method and application thereof. The multifunctional polymer is prepared by subjecting itaconic acid, 2-acrylamido-2-methylpropanesulfonic acid and tannic acid to oxidation and carrying out free radical polymerization. The multifunctional polymer has a structural formula shown in the description and has a molecular weight of four magnitudes. Through molecular design, massive hydroxyl groups are provided; coordinative aggregation of the various functional groups, such as carboxyl group, amido group, sulfo group, hydroxyl group and aromatic rings, is achieved; coaction of the groups gives rise to high hydrophilicity, adsorbing performance and scale-inhibiting performance; as a scale inhibitor, the multifunctional polymer helps effectively remove CaCO3 and CaSO4 scale and plays an important role of reducing operating cost of a reverse osmosis system and extending the life of equipment; the multifunctional polymer has excellent viscosity-reducing and dispersing properties; as a water-coal-slurry additive, the multifunctional polymer provides high concentration, low viscosityand good stability for the prepared water coal slurry. The invention also provides the preparation method and application of the multifunctional polymer.
Owner:SHANDONG UNIV OF TECH

Preparation method and application of magnesium-titanium co-doped cobalt carbonate

The invention discloses a preparation method and application of magnesium-titanium co-doped cobalt carbonate, a cobalt-magnesium mixed metal liquid, a precipitator solution and a titanium salt solution are added into a base solution in a parallel flow mode for a reaction, magnesium-titanium co-doped cobalt carbonate slurry is obtained, the precipitator solution is a mixed solution of carbonate and a surfactant, and the titanium salt solution is a mixed solution of magnesium carbonate and titanium carbonate. The titanium salt solution is a mixed solution of an acidic complexing agent and a titanium salt, then carrying out solid-liquid separation on the magnesium-titanium co-doped cobalt carbonate slurry, and washing and drying the obtained solid to obtain the magnesium-titanium co-doped cobalt carbonate. Titanium salt is independently fed into the solution, the acid complexing agent is added into the titanium salt solution, the effects of complexing titanium ions and inhibiting hydrolysis of titanium can be achieved at the same time, the surface active agent and the carbonate solution are mixed, the adsorption capacity of the surfaces of precursor secondary particle balls in the synthesis stage is improved, growth of magnesium-titanium co-doped cobalt carbonate is promoted, and the synthesis efficiency is improved. And the rate capability of the lithium cobalt oxide positive electrode material is remarkably improved by doping magnesium and titanium elements in the bulk phase.
Owner:GUANGDONG BRUNP RECYCLING TECH +1

Process system and method for refining dimethyl formamide serving as extraction solvent of C5 separation device

The invention relates to a process system and method for refining an extraction solvent dimethylformamide of a C5 separation device. The process system comprises the following steps: a solvent regeneration kettle carries out decoking treatment on the fed solvent dimethylformamide needing to be refined, and the decoked material is extracted from a gas phase, is condensed by a first condenser and then enters a crude solvent tank; conveying the crude solvent to a solvent refining tower by a crude solvent pump; the solvent refining tower, the second condenser, the reflux tank and the reflux pump of the solvent refining tower form a circulation loop, the solvent refining tower carries out reduced pressure rectification operation on a material subjected to coke removal, the material subjected to reduced pressure rectification is extracted from a gas phase and enters the reflux tank after being condensed by the second condenser, and azeotropic rectification is carried out by taking water as reflux liquid; hydrolysis inhibitor hydrocarbon substances are added into water and intermittently extracted from the tower top through azeotropy, materials subjected to azeotropic rectification are conveyed back to the solvent refining tower through a reflux pump of the solvent refining tower, and after multiple cycles, a tower kettle pump of the solvent refining tower is used for pumping out a refining solvent dimethylformamide, and a tower top extraction pump of the solvent refining tower is used for pumping out impurities.
Owner:CHINA PETROLEUM & CHEM CORP +1

Formula milk powder capable of maintaining bone health and increasing bone mineral substances, and preparation method

The invention discloses a formula milk powder capable of maintaining bone health and increasing bone mineral substances, and a preparation method, and belongs to a dairy product and a preparation technology. The formula milk powder is formed by the compatibility of raw material milk powder, colostrum basic protein and histidine according to parts by weight. Under a condition that a temperature is20-24 DEG C and humidity is 45-65%, the colostrum basic protein and the histidine, which are screened by a sieve of 120 meshes and are sterilized through ultraviolet rays, and 6-10% of the raw material milk powder are subjected to first-level pre-mixing in a three-dimensional mixer for 20-25 min; then, materials subjected to first-level pre-mixing are screened by a sieve of 40 meshes, then, the materials and 90-94% of the residual raw material milk powder are added into a high-speed mixer to be subjected to dry blending under a condition of 35-45 revolution/min for 200-250 S; then, materials subjected to secondary-level dry blending are sent into a packing machine to be vacuumized; and inert gas filling and packaging are carried out to obtain the formula milk powder. According to the formula milk powder, the bone health can be effectively maintained for a long time, effects on supplementing calcium and increasing mineral substances are good, the formula milk powder is safe to eat and has a simple production technology, and nutrient ingredient loss is small.
Owner:白永纯

Synergistic utilization of waste incineration fly ash and steel slag to prepare high-strength bricks

The invention discloses a method for synergistically utilizing waste incineration fly ash and steel slag to prepare high-strength bricks, comprising the following steps: (1) grinding steel slag to obtain steel slag powder; (2) grinding blast furnace slag to obtain blast furnace slag powder; (3) mixing steel slag powder, blast furnace slag powder, and fly ash to obtain fly ash intermixing powder; (4) mixing water and fly ash intermixing powder, stirring evenly, putting into a mold, and curing to obtain an anode assembly block; (5) ) mixing sodium phosphate and sodium silicate to obtain silicon phosphorus reagent; (6) mixing silicon phosphorus reagent with water, stirring until sodium phosphate and sodium silicate are completely dissolved to obtain silicon phosphorus solution; (7) adding ethanol to silicon phosphorus (8) connect the anode assembly block to the anode and soak in the electrolyte solution, connect the DC power supply, activate, remove the anode assembly block, and maintain it to obtain high-strength bricks. The process of the invention is simple, and can be operated under normal temperature environment to realize the conversion of waste incineration fly ash into high-strength bricks.
Owner:浙江中陶环保科技集团有限公司

Multifunctional polymer and its preparation method and application

The invention relates to a polymer compound, in particular to a multifunctional polymer and its preparation method and application. Taking itaconic acid, 2-acrylamido-2-methylpropanesulfonic acid and tannic acid as raw materials, carry out oxidation reaction and free radical polymerization to obtain multifunctional polymer; its structural formula is as follows: described multifunctional polymer The molecular weight is four orders of magnitude. Through molecular design, it contains a large number of hydroxyl groups, and at the same time realizes the coordinated aggregation of various functional groups such as carboxyl groups, amido groups, sulfonic acid groups, hydroxyl groups and aromatic rings. Through the joint action of each group, it has strong hydrophilicity, adsorption performance and Antiscalant properties, as an antiscalant, effectively eliminates CaCO 3 and CaSO 4 It plays an important role in reducing the operating cost of the reverse osmosis system and prolonging the life of the equipment; it has excellent viscosity reduction and dispersion properties, and as an additive for coal-water slurry, it makes the prepared coal-water slurry high in concentration, low in viscosity and good in stability; The invention also provides its preparation method and application.
Owner:SHANDONG UNIV OF TECH
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