Yi medicine polygonum persicaria extract as well as preparation method and anti-cancer application thereof
A technology of Polygonum serrata extract, which is applied in the field of Yi drug Polygonum serrata extract and its preparation, can solve problems such as research lag, achieve the effects of improving resource development, promoting development and utilization, and simplifying the preparation process
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Embodiment 1
[0038] Example 1 Preparation of different polarity extraction parts of Polygonum serrata tuber root
[0039] (1) Powder the hard root tubers of Polygonum serrata after drying in the shade, pass through a 40-mesh sieve, add 95% ethanol solution according to the material ratio of 1:20 (g / mL), stir well, and then room temperature (20±5°C) ) conditions soaked. During the immersion process, the infiltrated samples were thoroughly stirred every 4 hours for a total of 24 hours.
[0040] (2) Leave the ethanol extract obtained in step (1) until the liquid is clear, then filter the extract by pressure suction filtration, and repeat the suction filtration step 3 times until there is no medicinal residue.
[0041] (3) Steps (1) and (2) were repeated, and the roots of Polygonum serrata were soaked and extracted for 3 to 4 times for 24 hours, and all the extracts were collected.
[0042] (4) Concentrate the ethanol extract collected in step (3) under reduced pressure (temperature 45±5°C, ...
Embodiment 2
[0046] Example 2 Application of different extraction parts of Polygonum serrata root tuber in research and development of anticancer drugs
[0047] (1) Principle of MTS assay for cell viability
[0048] MTS is a brand new MTT analog, its full name is 3-(4,5-dimethylthiazol-2-yl)-5(3-carboxymethoxyphenyl)-2-(4-sulfopheny)-2H-tetrazolium, it is a yellow color of dyes. The succinate dehydrogenase in the mitochondria of living cells can metabolize and reduce MTS to generate soluble formazan (Formazan) compounds, and the content of formazan can be measured with a microplate reader at 490nm. Under normal circumstances, the amount of formazan produced is directly proportional to the number of living cells, so the number of living cells can be inferred from the optical density OD value.
[0049] (2) Experimental method
[0050] 1) Cell inoculation: Prepare a single cell suspension with culture medium (DMEM or RMPI1640) containing 10% fetal bovine serum, and inoculate into a 96-well...
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