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Insecticidal composition containing fluensulfone and allyl isothiocyanate

An insecticidal composition, a technology of isothiocyanate, applied in the field of pesticides, can solve the problems of high surface tension, difficult to wet and spread, poor dispersibility and the like

Inactive Publication Date: 2021-12-03
合肥巨卓农业科技合伙企业(有限合伙)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] (2) Add n-octane and n-octene in the three-necked flask, place the three-necked flask in the glove box and add zirconocene dichloride and methylaluminoxane to obtain intermediate B, and add intermediate B and Dimethyl phosphite, add catalyst, obtain intermediate D, add intermediate D, sodium hydroxide, distilled water and ethanol in the there-necked flask, obtain this wetting auxiliary agent, solve the large surface tension of existing pesticide, in application The dispersibility of the medicine is poor, and it is not easy to wet and spread on the leaf surface and root system of the target organism, which reduces the efficacy of the medicine

Method used

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  • Insecticidal composition containing fluensulfone and allyl isothiocyanate
  • Insecticidal composition containing fluensulfone and allyl isothiocyanate
  • Insecticidal composition containing fluensulfone and allyl isothiocyanate

Examples

Experimental program
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Effect test

Embodiment 1

[0036] This embodiment is an insecticidal composition containing fluorine sulfone and allyl isothiocyanate, including the following components in parts by weight:

[0037] 30 parts of sulfone, 20 parts of allyl isothiocyanate, 5 parts of stabilizing aid, 5 parts of wetting aid, 20 parts of filler or solvent;

[0038] Wherein the stabilizing aid is prepared by the following steps:

[0039] S1: adding chloroplatinic acid into isopropanol, stirring and dissolving to obtain a catalyst;

[0040] S2: Add allyl glycidyl ether and catalyst to a three-neck flask equipped with a nitrogen device, a reflux condensing device and a constant pressure dropping funnel. After heating to 80°C, add a toluene solution containing hydrogen silicone oil dropwise to control the dropping rate 1 drop / s, reacted for 4 hours under the protection of nitrogen, distilled under reduced pressure, precipitated three times in a mixture of n-hexane and tetrahydrofuran with a volume ratio of 20 / 1, and placed it i...

Embodiment 2

[0048] This embodiment is an insecticidal composition containing fluorine sulfone and allyl isothiocyanate, including the following components in parts by weight:

[0049] 30 parts of sulfone, 20 parts of allyl isothiocyanate, 4 parts of stabilizing aid, 5 parts of wetting aid, 3 parts of filler or solvent;

[0050] Wherein the stabilizing aid is prepared by the following steps:

[0051] S1: adding chloroplatinic acid into isopropanol, stirring and dissolving to obtain a catalyst;

[0052] S2: Add allyl glycidyl ether and catalyst to a three-neck flask equipped with a nitrogen device, a reflux condensing device and a constant pressure dropping funnel. After heating to 80°C, add a toluene solution containing hydrogen silicone oil dropwise to control the dropping rate 1 drop / s, reacted for 4 hours under the protection of nitrogen, distilled under reduced pressure, precipitated three times in a mixture of n-hexane and tetrahydrofuran with a volume ratio of 20 / 1, and placed it in...

Embodiment 3

[0060] This embodiment is an insecticidal composition containing fluorine sulfone and allyl isothiocyanate, including the following components in parts by weight:

[0061] 40 parts of sulfone, 10 parts of allyl isothiocyanate, 6 parts of stabilizing aid, 4 parts of wetting aid, 30 parts of filler or solvent;

[0062] Wherein the stabilizing aid is prepared by the following steps:

[0063] S1: adding chloroplatinic acid into isopropanol, stirring and dissolving to obtain a catalyst;

[0064] S2: Add allyl glycidyl ether and catalyst to a three-necked flask equipped with a nitrogen device, a reflux condensing device and a constant pressure dropping funnel. After heating to 90°C, add a toluene solution containing hydrogen silicone oil dropwise to control the dropping rate 2 drops / s, reacted for 5 hours under the protection of nitrogen, distilled under reduced pressure, precipitated 4 times in the mixture of n-hexane and tetrahydrofuran with a volume ratio of 20 / 1, and placed it ...

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PUM

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Abstract

The invention discloses an insecticidal composition containing fluensulfone and allyl isothiocyanate, and relates to the field of pesticides. Chloroplatinic acid is added into isopropanol to obtain a catalyst, allyl glycidyl ether and the catalyst are added into a three-necked flask, a toluene solution containing hydrogen silicone oil is dropwise added to obtain an intermediate A, the intermediate A and polyether amine are added into the three-necked flask, ethanol is added as a solvent, a stabilizing aid is obtained; the stabilizing aid is added into the composition, the problems that foams are easily generated in the dilution process of the existing pesticide, the dispersion uniformity of the pesticide is reduced, the pesticide effect is influenced and the spraying operation is interfered are solved; the amino group is introduced, so that the hydrophilicity is increased, and the amino group can be ionized, is positively charged, has a good bubble breaking effect on a negatively charged bubble film, remarkably reduces the surface tension, enables a pesticide to be quickly spread, wet and permeate on the surface of a plant, and enables the pesticide to exert higher efficiency, thereby achieving the purpose of reducing the generation of bubbles.

Description

technical field [0001] The invention relates to the field of pesticides, in particular to an insecticidal composition containing fluorine sulfone and allyl isothiocyanate. Background technique [0002] Plant nematode disease is a plant disease caused by the invasion and parasitism of plant parasitic nematodes. The normal growth and development of the damaged plants are affected by the invading nematodes absorbing nutrients in the body. The secretions of the nematodes in the metabolic process will stimulate the cells and tissues of the host plant, resulting in plant deformities , so that the production and quality of agricultural products are reduced. At present, the more serious plant nematode diseases include root-knot nematode disease of peanuts and other crops, soybean cyst nematode disease, wheat grain nematode disease, sweet potato stem nematode disease and rice stem nematode disease, etc. Plant parasitic nematodes are mostly linear, colorless or milky white, without se...

Claims

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Application Information

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IPC IPC(8): A01N43/78A01N47/46A01P7/04
CPCA01N43/78A01N47/46
Inventor 刘言合陈琦
Owner 合肥巨卓农业科技合伙企业(有限合伙)
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