Insecticidal composition containing fluensulfone and allyl isothiocyanate
An insecticidal composition, a technology of isothiocyanate, applied in the field of pesticides, can solve the problems of high surface tension, difficult to wet and spread, poor dispersibility and the like
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Embodiment 1
[0036] This embodiment is an insecticidal composition containing fluorine sulfone and allyl isothiocyanate, including the following components in parts by weight:
[0037] 30 parts of sulfone, 20 parts of allyl isothiocyanate, 5 parts of stabilizing aid, 5 parts of wetting aid, 20 parts of filler or solvent;
[0038] Wherein the stabilizing aid is prepared by the following steps:
[0039] S1: adding chloroplatinic acid into isopropanol, stirring and dissolving to obtain a catalyst;
[0040] S2: Add allyl glycidyl ether and catalyst to a three-neck flask equipped with a nitrogen device, a reflux condensing device and a constant pressure dropping funnel. After heating to 80°C, add a toluene solution containing hydrogen silicone oil dropwise to control the dropping rate 1 drop / s, reacted for 4 hours under the protection of nitrogen, distilled under reduced pressure, precipitated three times in a mixture of n-hexane and tetrahydrofuran with a volume ratio of 20 / 1, and placed it i...
Embodiment 2
[0048] This embodiment is an insecticidal composition containing fluorine sulfone and allyl isothiocyanate, including the following components in parts by weight:
[0049] 30 parts of sulfone, 20 parts of allyl isothiocyanate, 4 parts of stabilizing aid, 5 parts of wetting aid, 3 parts of filler or solvent;
[0050] Wherein the stabilizing aid is prepared by the following steps:
[0051] S1: adding chloroplatinic acid into isopropanol, stirring and dissolving to obtain a catalyst;
[0052] S2: Add allyl glycidyl ether and catalyst to a three-neck flask equipped with a nitrogen device, a reflux condensing device and a constant pressure dropping funnel. After heating to 80°C, add a toluene solution containing hydrogen silicone oil dropwise to control the dropping rate 1 drop / s, reacted for 4 hours under the protection of nitrogen, distilled under reduced pressure, precipitated three times in a mixture of n-hexane and tetrahydrofuran with a volume ratio of 20 / 1, and placed it in...
Embodiment 3
[0060] This embodiment is an insecticidal composition containing fluorine sulfone and allyl isothiocyanate, including the following components in parts by weight:
[0061] 40 parts of sulfone, 10 parts of allyl isothiocyanate, 6 parts of stabilizing aid, 4 parts of wetting aid, 30 parts of filler or solvent;
[0062] Wherein the stabilizing aid is prepared by the following steps:
[0063] S1: adding chloroplatinic acid into isopropanol, stirring and dissolving to obtain a catalyst;
[0064] S2: Add allyl glycidyl ether and catalyst to a three-necked flask equipped with a nitrogen device, a reflux condensing device and a constant pressure dropping funnel. After heating to 90°C, add a toluene solution containing hydrogen silicone oil dropwise to control the dropping rate 2 drops / s, reacted for 5 hours under the protection of nitrogen, distilled under reduced pressure, precipitated 4 times in the mixture of n-hexane and tetrahydrofuran with a volume ratio of 20 / 1, and placed it ...
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