The invention belongs to the technical field of
chemical synthesis, and particularly relates to a synthesis method of a self-foaming type
sulfide ore flotation collecting agent. The synthesis method comprises the following steps: by taking
allyl isothiocyanate and
isooctyl alcohol polyoxyethylene ether as raw materials, under the action of an esterification catalyst, carrying out a heating
reflux reaction, and removing unreacted
isooctyl alcohol polyoxyethylene ether under reduced pressure, so as to prepare N-allyl-O-isooctyl
polyoxyethylene ether-thionocarbamate; by adopting the high-boiling-point
raw material, the problems of low conversion rate and high toxic
raw material residue caused by limited
reaction temperature in the traditional process are solved, and the obtained product is high in purity, has excellent collecting and foaming functions, is relatively long in hydrophobic chain, and can remarkably reduce the consumption of a
foaming agent and the COD value of
wastewater in the flotation process; the synthesis method provided by the invention has the advantages of simple process, controllable reaction, high safety and easiness in industrial production.