Antibacterial master batch, polyester DTY (Draw Textured Yarn) using antibacterial master batch and production method of polyester DTY
An antibacterial masterbatch and polyester technology, which is applied in the textile field, can solve the problems of easy breeding of microorganisms, easy contamination of fiber products, affecting the use of textiles, etc., and achieves good antibacterial effect, good mechanical properties and antibacterial properties, and improves the effect of stability.
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preparation example Construction
[0037] The antibacterial masterbatch mentioned in this embodiment is prepared by a preparation method of an antibacterial masterbatch in the present application, and the preparation method of the antibacterial masterbatch specifically includes the following steps:
[0038]Modification treatment: use silane coupling agent to modify nano-silica, filter and dry to obtain modified nano-silica;
[0039] Loading and coating: add dispersant in water, mix and stir modified nano-silica and nano-silver in water, filter and dry to obtain nano-silver carrier; then add dispersant and silane coupling agent, mix and stir nano-silver Carrier and PVC paste resin to obtain the coated nano-silver carrier;
[0040] Mixing extrusion: add silane coupling agent, mix and stir the coated nano-silver carrier and polyester resin, melt extrusion and granulate to obtain antibacterial masterbatch.
[0041] There is no particular limitation on the fiber-grade polyester chips mentioned in this embodiment, a...
preparation example 1
[0051] An antibacterial masterbatch, including the following components: 0.33kg of nano-silver, 0.85kg of nano-silica, 1.55kg of silane coupling agent, 4.2kg of dispersant, 83kg of polyester resin, and 10kg of PVC paste resin.
[0052] Among them, the silane coupling agent is KH-550;
[0053] The dispersant is sodium hexametaphosphate;
[0054] The preparation method of this antibacterial master batch comprises the following steps:
[0055] S1 modification treatment: Divide the silane coupling agent into three parts according to the mass ratio of 2:1:1, mix and stir nano-silica and 1 / 2 the amount of silane coupling agent, mix and stir for 30 minutes, then let it stand for 1 hour, keep The temperature is 40°C, modify the nano-silica, and then filter and dry the nano-silica, the drying temperature is 90°C, and the drying time is 40min, to obtain the modified nano-silica;
[0056] S2 load-bearing coating: add half of the amount of dispersant in water, and mix and stir the modif...
preparation example 6
[0061] The difference between this preparation example and preparation example 1 is that no nano silicon dioxide is added.
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