Graphene hot compress material for eye massager and preparation method of graphene hot compress material
A graphene and massager technology, which is applied in the field of graphene hot compress materials and its preparation, can solve problems such as insufficient stability of electrothermal conversion effect, high risk of eye health care, and large safety problems, and achieve excellent electrothermal conversion effect and mechanical properties and thermal conductivity improvement, the effect of safe use
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Embodiment 1
[0038] A kind of preparation method of the graphene hot compress material that is used for eye massager, concrete steps are as follows:
[0039] (1) First, graphite oxide and tributylethylphosphine bis(trifluoromethanesulfonyl)imide salt are used as raw materials, and the doped graphene oxide is obtained through hydrothermal reaction; then with a volume concentration of 70% ethanol aqueous solution as a solvent, Partially reducing the doped graphene oxide to prepare solution I, then adding fatty acid and ethyl orthosilicate to solution I, stirring and reacting under nitrogen atmosphere to obtain solution II;
[0040] (2) Then add styrene and potassium persulfate to solution II, polymerize under a nitrogen atmosphere, and centrifuge to obtain composite microspheres;
[0041] (3) Ultrasonic disperse the composite microspheres in deionized water, add formaldehyde, phenol and ammonia solution, react with microwave irradiation, centrifuge, wash, and dry to obtain modified microsphere...
Embodiment 2
[0058] A kind of preparation method of the graphene hot compress material that is used for eye massager, concrete steps are as follows:
[0059] (1) First, using graphite oxide and tributylethylphosphine bis(trifluoromethanesulfonyl)imide salt as raw materials, hydrothermal reaction makes doped graphene oxide; then with volume concentration 80% ethanol aqueous solution as solvent, Partially reducing the doped graphene oxide to prepare solution I, then adding fatty acid and ethyl orthosilicate to solution I, stirring and reacting under nitrogen atmosphere to obtain solution II;
[0060] (2) Then add styrene and potassium persulfate to solution II, polymerize under a nitrogen atmosphere, and centrifuge to obtain composite microspheres;
[0061] (3) Ultrasonic disperse the composite microspheres in deionized water, add formaldehyde, phenol and ammonia solution, react with microwave irradiation, centrifuge, wash, and dry to obtain modified microspheres, and then ultrasonically dis...
Embodiment 3
[0078] A kind of preparation method of the graphene hot compress material that is used for eye massager, concrete steps are as follows:
[0079] (1) First, using graphite oxide and tributylethylphosphine bis(trifluoromethanesulfonyl)imide salt as raw materials, hydrothermal reaction makes doped graphene oxide; then with volume concentration 75% ethanol aqueous solution as solvent, Partially reducing the doped graphene oxide to prepare solution I, then adding fatty acid and ethyl orthosilicate to solution I, stirring and reacting under nitrogen atmosphere to obtain solution II;
[0080] (2) Then add styrene and potassium persulfate to solution II, polymerize under a nitrogen atmosphere, and centrifuge to obtain composite microspheres;
[0081] (3) Ultrasonic disperse the composite microspheres in deionized water, add formaldehyde, phenol and ammonia solution, react with microwave irradiation, centrifuge, wash, and dry to obtain modified microspheres, and then ultrasonically dis...
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