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TLC identification and hplc detection method of burrowing wind in Henggu bone wound healing agent

A Henggu bone healing and detection method technology, which is applied in the fields of TLC identification and HPLC detection, can solve the problems of ineffective detection of active ingredients, etc., and achieve the effect of simple test method, improved accuracy, and improved detection accuracy

Active Publication Date: 2022-03-25
赛灵药业科技集团股份有限公司
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Problems solved by technology

[0008] Therefore, the present invention provides a method for TLC identification and HPLC detection of earth-boring wind in Henggu bone healing agent, to overcome the problem that the active ingredients in Chinese patent medicines cannot be accurately and efficiently detected in the prior art

Method used

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  • TLC identification and hplc detection method of burrowing wind in Henggu bone wound healing agent
  • TLC identification and hplc detection method of burrowing wind in Henggu bone wound healing agent
  • TLC identification and hplc detection method of burrowing wind in Henggu bone wound healing agent

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Embodiment 1

[0075] see figure 1 Shown, it is the TLC identification method detection flowchart of the present invention, and its steps include:

[0076] Step S1, the TLC identification process of the ground-drilling wind medicinal material in Henggu Orthopedic Wound Healing Agent:

[0077] Step S11, preparing a rosinic acid reference solution, taking an appropriate amount of rosinic acid isolated from the earth-boring wind medicinal material, adding methanol to dissolve, and preparing a solution with a concentration of 1.95 mg / mL as a reference solution;

[0078] Step S12, preparing the earth-boring wind medicinal material solution, taking 2 g of each of the three batches of earth-boring wind medicinal materials, adding 30 ml of chloroform-methanol 1:1 solution, ultrasonic treatment for 30 minutes, filtering, and evaporating the filtrate to dryness, adding 5 ml of methanol to the residue to dissolve, as Earth-burrowing wind medicinal solution;

[0079] Step S13, prepare the test solutio...

Embodiment 2

[0092] see figure 1 Shown, it is the TLC identification method detection flowchart of the present invention, and its steps include:

[0093] Step S1, the TLC identification process of the ground-drilling wind medicinal material in Henggu Orthopedic Wound Healing Agent:

[0094] Step S11, preparing a rosinic acid reference solution, taking an appropriate amount of rosinic acid isolated from the earth-boring wind medicinal material, adding methanol to dissolve, and preparing a solution with a concentration of 1.95 mg / mL as a reference solution;

[0095] Step S12, preparing the earth-boring wind medicinal material solution, taking 2 g of each of the three batches of earth-boring wind medicinal materials, adding 30 ml of chloroform-methanol 1:1 solution, ultrasonic treatment for 30 minutes, filtering, and evaporating the filtrate to dryness, adding 5 ml of methanol to the residue to dissolve, as Earth-burrowing wind medicinal solution;

[0096] Step S13, prepare the test solutio...

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Abstract

The invention discloses a method for TLC identification and HPLC detection of earth-boring wind in Henggu bone wound healing agent, comprising: a preparation method of a reference substance solution, a preparation method of a reference medicinal material solution, a preparation method of a test sample solution, a preparation method of a negative control solution, Determine the color development conditions for sample point development, determine the chromatographic conditions, develop, HPLC sample injection detection, perform quantitative detection, read and record data, and perform data analysis; it can detect the parameters of the earth-penetrating wind in Henggu bone wound healing agent, which is very important for healing The quality of the agent is controlled; the TLC identification equipment is equipped with a central control processor to receive and analyze the scan data, and the detection adjustment parameters are set in the central control processor to adjust the TLC identification equipment during detection, which improves the Detection accuracy; TLC identification equipment also includes a workbench, toggle and limit frame, which are used to fix the thin-layer board to be tested to prevent the displacement of the thin-layer board during detection, and further improve the detection efficiency and accuracy.

Description

technical field [0001] The invention relates to the technical field of TLC identification and HPLC detection methods, in particular to a TLC identification and HPLC detection method of earth-boring wind in Henggu bone wound healing agent. Background technique [0002] Fractures, femoral head necrosis, and lumbar disc herniation have remained high in incidence in my country, and have become one of the major diseases that threaten public health and life in my country. Most patients with femoral head necrosis are between 30 and 50 years old. With increasing age, the incidence rate showed a gradual increasing trend. The occurrence of lumbar disc herniation is mainly closely related to factors such as intervertebral disc degeneration, injury, pregnancy, heredity, and abnormal development. Lumbar trauma and improper posture can also cause lumbar keyboard herniation. It is more likely to occur in young adults, people with poor working posture, pregnant women and menopausal women, e...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90G01N30/95G01N30/02G01N30/06G01N30/86
CPCG01N30/90G01N30/95G01N30/02G01N30/06G01N30/8675G01N2030/047
Inventor 易志恒王飘曹智刚
Owner 赛灵药业科技集团股份有限公司
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