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Additive manufacturing powder core wire material preparation method for obtaining alloy with accurate components by regulating and controlling powder particle size

A powder core wire material and additive manufacturing technology, which is applied in the field of powder core wire materials for metal additive manufacturing and powder core wire materials for additive manufacturing, can solve the problem that the alloy cannot obtain the expected composition, etc. Achieve the effect of high practical application value, convenient and quick method, and broaden the research field and application field

Active Publication Date: 2022-06-17
JIANGSU UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] The purpose of the present invention is to solve the problem of "the burning loss of different elements is different in the additive manufacturing process, resulting in the alloy prepared by additive manufacturing can not obtain the expected composition", combining the powder of the same element under the same heat input conditions The melting and boiling points of different particle sizes, especially at the nanometer level, are characterized by large differences, and the powder core of the powder core wire has a pore structure that has thermal resistance, which can make the easily burnable element powder in a relatively low temperature state. It is proposed to control the powder The size of the particle size is used to control the burning loss of different powders in the powder core wire, so that the prepared alloy can obtain the composition that meets the design expectations. A powder core wire for additive manufacturing that obtains an alloy with accurate composition by adjusting the particle size of the powder Material matching method

Method used

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  • Additive manufacturing powder core wire material preparation method for obtaining alloy with accurate components by regulating and controlling powder particle size
  • Additive manufacturing powder core wire material preparation method for obtaining alloy with accurate components by regulating and controlling powder particle size
  • Additive manufacturing powder core wire material preparation method for obtaining alloy with accurate components by regulating and controlling powder particle size

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0047] like Figure 1-3 shown.

[0048] Taking the preparation of 83Cu-13Al-4Fe alloy powder core wire as an example, the boiling point of Cu is 2562 °C, the boiling point of Al is 2327 °C, and the boiling point of Fe is 2750 °C. It can be seen that the boiling point of Al is the lowest (2327 °C), so the Al element is easy to burn Loss elements (need to increase particle size), and Cu element is selected as the object to reduce particle size.

[0049] Step 1: According to figure 1 The relationship curve between the Cu element powder and the boiling point and melting point, the angle between the tangent of the point on the curve 1 and the nominal boiling point of the element is equal to 5° to distinguish the growth segment and the flat segment, and the corresponding particle size at the junction of the growth segment and the flat segment is 60nm. As the preferred particle size of the Cu element powder (indicated by the vertical dotted line in the figure), then the 60nm partic...

example 2

[0059] Taking the preparation of 84Cu-14Al-2Mn alloy powder core wire as an example, the boiling point of Cu is 2562 °C, the boiling point of Al is 2327 °C, and the boiling point of Mn is 1962 °C. It can be seen that the boiling point of Mn is the lowest (1962 °C), so the Mn element is easy to burn Loss elements (need to increase particle size), and Cu element is selected as the object to reduce particle size.

[0060] Step 1: According to the relationship curve between Cu element powder and boiling point and melting point, take the angle between the tangent of the point on the curve and the nominal boiling point of the element equal to 5° as the boundary to distinguish the growth section and the flat section, and select the corresponding point at the junction of the growth section and the flat section. The particle size of 60nm is used as the preferred particle size of Cu element powder, and then the 60nm particle size of Cu powder is used as the benchmark to decrease in order...

example 3

[0070] Taking the preparation of 66Fe-14Mn-6Si-9Cr-5Ni alloy powder core wire as an example, the boiling point of Fe is 2750 °C, the boiling point of Mn is 1962 °C, the boiling point of Si is 2355 °C, the boiling point of Cr is 2672 °C, and the boiling point of Ni is 2730 °C , it can be seen that the boiling point of Mn is the lowest, so the Mn element is an element that is easy to burn (need to increase the particle size), and Fe and Ni elements are selected as the objects to reduce the particle size. It should be noted in this example that, considering that the boiling points of Fe element and Ni element are basically the same, it is regarded as an element (defined as Fe / Ni element in this example) for regulation, and considering that the content of Fe element in the wire of this system is It can be used as the outer skin at most, so the mass fraction of Fe powder contained in the powder core can be the same as the Ni element.

[0071] Step 1: According to the relationship b...

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Abstract

The invention relates to a powder core wire material preparation method (taking preparation of element alloy as an example) for additive manufacturing, and the powder core wire material preparation method is characterized in that an alphaC1-CbetaC2-gammaC3 ternary alloy powder core wire material is prepared, alpha, beta and gamma are mass fractions of elements C1, C2 and C3 respectively, and the sum of alpha, beta and gamma is 100%; wherein the element C1 is the element with the highest mass fraction in the alloy, the element C2 is the easily burnt element, namely the element with the lowest boiling point in the alloy, and a seamless round pipe or strip which contains all or part of the alloy elements in the market and takes the element C1 with the highest mass fraction as the main component is selected as the outer skin of the cored wire. The mass of the elements except the mass of the elements C1, C2 and C3 contained in the outer skin serves as the filling amount of the powder core needing to be filled, the powder particle size of the element C1 or (and) C3 is reduced, the powder particle size of the element C2 easy to burn out is increased, and therefore the powder core wire additive manufacturing alloy accurate in component is obtained by adjusting and controlling the powder particle size.

Description

technical field [0001] The invention relates to a method for preparing a material for metal additive manufacturing, in particular to a method for preparing a powder core wire for metal additive manufacturing, in particular to an additive for obtaining an alloy with accurate composition by regulating the particle size of the powder A method of manufacturing powder core wire materials. Background technique [0002] Metal additive manufacturing is an important part of the field of additive manufacturing. At present, the commonly used materials for metal additive manufacturing are powder and wire, and wire can be divided into solid wire and powder core wire. Among them, the powder core wire is a new material for additive manufacturing that uses a metal tube or strip as the outer skin to wrap the powder and reduce the diameter and draw it into a wire. Powder core wire not only avoids the disadvantage of low material utilization rate of powder in the additive manufacturing proce...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C9/01B22F10/28B22F10/20C22C38/34C22C38/58B33Y10/00B33Y70/00
CPCC22C9/01B22F10/28B22F10/20C22C38/34C22C38/58B33Y10/00B33Y70/00Y02P10/25
Inventor 王宏宇唐第东陈胜袁晓明杨杰黄金雷朱长顺张秦
Owner JIANGSU UNIV