Adhesive composition for optical component and binding film for optical component therewith
A technology for optical components and adhesives, applied in adhesive types, ester copolymer adhesives, film/sheet adhesives, etc., can solve problems such as slow crosslinking reactions
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manufacture example 1
[0027] Acrylic polymer solution A
[0028]Put 100 parts by weight of n-butyl acrylate, 4 parts by weight of 2-hydroxyethyl acrylate, 0.5 parts by weight of acrylic acid, 90 parts by weight of ethyl acetate and 0.1 parts by weight of benzoyl peroxide into the reactor, and replace the air in the reactor. Then, it heated up to 70 degreeC, stirring, and it reacted for 8 hours, and the acrylic polymer solution A was obtained. The obtained acrylic polymer A had a Mw of 1.2 million as measured by GPC.
manufacture example 2
[0029] Acrylic polymer solution B
[0030] Put 100 parts by weight of n-butyl acrylate, 2 parts by weight of 2-hydroxyethyl acrylate, 1 part by weight of acrylamide, 100 parts by weight of ethyl acetate and 0.2 parts by weight of azobisisobutyronitrile into the reactor, and use nitrogen gas to The air in the reactor was replaced. Then, the temperature was raised to 60°C while stirring, and the reaction was carried out for 4 hours. After 4 hours, 100 parts by weight of toluene, 5 parts by weight of α-methylstyrene dimer, and 2 parts by weight of azobisisobutyronitrile were added, and the temperature was raised. The temperature was increased to 90° C., and the reaction was further carried out for 4 hours to obtain an acrylic polymer solution B. The obtained acrylic polymer B had a Mw of 700,000 as measured by GPC.
manufacture example 3
[0031] Acrylic polymer solution C
[0032] Put 100 parts by weight of 2-ethylhexyl acrylate, 0.5 parts by weight of 4-hydroxybutyl acrylate, 2.5 parts by weight of acrylamide, 90 parts by weight of ethyl acetate and 0.07 parts by weight of benzoyl peroxide into the reactor , replace the air in the reactor with nitrogen. Then, it heated up to 73 degreeC, stirring, and it reacted for 8 hours, and the acrylic polymer solution C was obtained. The obtained acrylic polymer C had a Mw of 1.4 million as measured by GPC.
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Abstract
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