Nonaqueous electrolyte secondary battery
A non-aqueous electrolyte and secondary battery technology, applied in the direction of non-aqueous electrolyte batteries, secondary batteries, organic electrolyte batteries, etc., can solve the problems of SEI deterioration, damage to the stability of the negative electrode, etc.
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Embodiment 1
[0214]
[0215] Lithium cobalt oxide (LixCoO 2 : but X is 03 positive pole.
[0216]
[0217] As the carbonaceous material A, the mesophase pitch-based carbon fiber (fiber diameter 8 μm, average fiber length 20 μm, length-to-diameter ratio 0.4, and powder X-ray diffraction) obtained by powder X-ray diffraction of the mesophase pitch-based carbon fiber (d 002 )0.3360nm, specific area measured by BET method 1m 2 / g) powder 89% by weight (95 parts by weight), and as the carbonaceous material B, the mesophase pitch-based carbon fiber (fiber diameter 8 μm, average fiber length 20 μm, length-to-diameter ratio 0.4, powder X-ray diffraction The surface spacing (d 002 )0.360nm, specific surface area measured by BET method 2.5m 2 / g) powder 4% by weight (5 parts by weight) is mixed, and then polyvinylidene fluoride (PVdF) 7% by weight and N-methyl-2-pyrrolidone (NMP) are mixed as a binder to prepare Slurry, the slurry is coated on both sides of the current collector made of copp...
Embodiment 2
[0230] Except that the proportion of carbonaceous material A and carbonaceous material B is 92 parts by weight of carbonaceous material A and 8 parts by weight of carbonaceous material B, other non-aqueous electrolyte secondary batteries are manufactured in the same manner as in Example 1 above.
Embodiment 3
[0232] The interplanar spacing (d 002 )0.3363nm, the specific surface area measured by BET method is 0.9m 2 / g) powder gets 89% by weight (95 parts by weight) and the mesophase pitch-based carbon fiber (fiber radius 8 μm, average fiber length 20 μm, powder X-ray diffraction) as carbonaceous material B through 700 ℃ of heat treatment ( 002) surface spacing (d 002 )0.36nm, the specific surface area measured by BET method is 2.5m 2 / g) powder is mixed with 4% by weight (5 parts by weight), and then mixed with 7% by weight of polyvinylidene fluoride (PVdF) and N-methyl-2-pyrrolidone (NMP) as a binder, Make a slurry, apply the slurry on both sides of a current collector composed of copper foil with a thickness of 12 μm, and dry and press to make an electrode with a density of 1.33g / cm 3 the negative pole.
[0233] Except for using this negative electrode, a nonaqueous electrolyte secondary battery was assembled in the same manner as in the above-mentioned embodiment.
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Abstract
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