Process for preparing Tibet medicine
A technology of medicinal residues and volatile oil, which is applied in pharmaceutical formulations, medical preparations containing active ingredients, and drug combinations, etc., can solve the problems of inconvenience, irritation, hygroscopicity, increased chemical activity, and decreased drug stability.
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Embodiment 1
[0096] Pomegranate seeds 326g Piper longum 32.6g Cinnamon 52g
[0097] Safflower 163g Cardamom 26g
[0098] Grind longicorns into fine powder, sieve, and set aside. Cinnamon and cardamom are used to extract the volatile oil by steam distillation, and the distilled aqueous solution is filtered, and the filtrate and residue are collected separately for later use. The pomegranate seed and safflower were refluxed and extracted three times with 80% ethanol, and the extraction time was 60 minutes, 40 minutes and 40 minutes respectively. Filtrate, combine the filtrates, recover ethanol and concentrate under reduced pressure to a clear paste with a relative density of about 1.10 (at room temperature). Combine the dregs extracted by ethanol with the dregs extracted from the volatile oil, add water to decoct twice, the first time for 80 minutes, the second time for 30 minutes, filter, the filtrate is combined with the filtrate extracted from the volatile oil, and concentrated to a...
Embodiment 2
[0100] Pomegranate seeds 326g Piper longum 32.6g Cinnamon 52g
[0101] Safflower 163g Cardamom 26g
[0102] Grind longicorns into fine powder, sieve, and set aside. Cinnamon and cardamom are used to extract the volatile oil by steam distillation, and the distilled aqueous solution is filtered, and the filtrate and residue are collected separately for later use. The volatile oil was mixed with a saturated aqueous solution of β-cyclodextrin, stirred evenly, refrigerated overnight, filtered, and dried. The pomegranate seeds and safflower were refluxed and extracted twice with 85% ethanol, and the extraction time was 60 minutes and 40 minutes respectively. Filtrate, combine the filtrates, recover ethanol and concentrate under reduced pressure to a clear paste with a relative density of about 1.10 (at room temperature). Combine the dregs extracted by ethanol with the dregs extracted from the volatile oil, add water to decoct twice, the first time for 60 minutes, the second...
Embodiment 3
[0104] Pomegranate seeds 326g Piper longum 32.6g Cinnamon 52g
[0105] Safflower 163g Cardamom 26g
[0106] Grind longicorns into fine powder, sieve, and set aside. Cinnamon and cardamom are used to extract the volatile oil by steam distillation, and the distilled aqueous solution is filtered, and the filtrate and residue are collected separately for later use. The volatile oil was mixed with a saturated aqueous solution of β-cyclodextrin, stirred evenly, refrigerated overnight, filtered, and dried. The pomegranate seeds and safflower were refluxed and extracted twice with 75% ethanol, and the extraction time was 90 minutes and 50 minutes respectively. Filtrate, combine the filtrates, recover ethanol and concentrate under reduced pressure to a clear paste with a relative density of about 1.10 (at room temperature). Merge the medicinal residues after ethanol extraction and the medicinal residues after extracting the volatile oil, add water to decoct twice, the first time...
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