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Cellulose base particle or liquid and their preparation and use method

A cellulose polymer and cellulose technology, applied in the field of ethyl cellulose and hydroxypropyl cellulose, preparation and use of the composition, can solve problems such as difficult to handle, unusable products, difficult to clean up, etc.

Inactive Publication Date: 2004-10-06
INTERNATIONAL FLAVORS & FRAGRANCES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Difficult to handle and especially difficult to clean up, making these products unusable

Method used

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  • Cellulose base particle or liquid and their preparation and use method
  • Cellulose base particle or liquid and their preparation and use method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0060] Hydroxypropyl Cellulose Extrudates

[0061] components

weight%

Mannitol, powder

67

KLUCEL GF

8

mint spice

25

[0062] step:

[0063] 1. Add Mannitol and KLUCEL to blender.

[0064] 2. Mix for 5 minutes.

[0065] 3. With the blender running, slowly add the flavor to the powder.

[0066] 4. Mix for 5-8 minutes.

[0067] 5. Mill the product to remove lumps.

[0068] 6. Add the powder blend to the extruder.

[0069] 7. Reduce the size of the extrudate by milling.

[0070] Extrusion conditions: (Werner & Pfleiderer ZSJ extruder)

[0071] Feeding speed

20 lbs / hour

screw speed

400RPM

Area temperature (℃)

0-0-90-90-90

Module (°C)

90

Die diameter

1.6mm

[0072] result:

[0073] The product is evenly fed and extruded to form a fine strand. The strands can be ground with dry ice to form small particles.

[0074] When placed in a t...

Embodiment 2

[0076] Hydroxypropyl Cellulose Extrudates

[0077] components

weight%

Hydrophobic silica, Syloid D11

10

KLUCEL GF

50

fragrance

40

[0078] step:

[0079] 1. Add Syloid and KLUCEL to blender.

[0080] 2. Mix until smooth.

[0081] 3. With the blender running, slowly add the fragrance to the powder.

[0082] 4. Mix until flowable.

[0083] 5. Add the powder blend to the extruder.

[0084] 6. Reduce the size of the extrudate by chopping.

[0085] Extrusion conditions: (Haake Lab extruder)

[0086] Feeding speed

overflow

screw speed

50-60RPM

Area temperature (℃)

70-85

Module (°C)

70-85

Die diameter

1 mm

[0087] result:

[0088] The product is evenly fed and extruded to form a fine strand. The strands were shredded by hand into small particles. They dissolve slowly when placed in cold water. In hot water, the particles retain thei...

Embodiment 3

[0090] breathable film

[0091] The materials in the following table were mixed using a Waring laboratory blender:

[0092] a

b

c

d

components

share(%)

share(%)

share(%)

share(%)

total water

77.98

77.98

77.93

77.70

cold water

46.79

46.79

46.76

46.62

hot water

31.19

31.19

31.17

31.08

Sweetener (Ace-K / Sucralose)

0.25

0.25

0.25

0.25

Purity Gum 59

12

12

12

12

HPMC E50

3

3

3

3

KelGum GFS

1

1

1

1

Glycerin

3

3

3

3

TWEEN 80

0.25

0.25

0.25

0.25

Menthol

2.52

--

--

--

Menthol Peppermint

--

2.52

--

-- ...

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Abstract

A particle composition containing a continuous phase of 0.5-95% organically soluble cellulosic material selected from the group consisting of ethyl cellulose and hydroxypropyl cellulose dissolved in 5-99.5% organic fragrance chemicals and organic flavor chemicals. The particles are formed from a continuous phase product that results from dissolving the cellulosic material in the flavor / fragrance which is subsequently subjected to techniques to form the desired particle size. Methods of making and using the particles are also disclosed.

Description

field of invention [0001] The present invention relates to compositions comprising organically compatible cellulosic materials, especially ethylcellulose and hydroxypropylcellulose capable of forming substantially continuous solutions with flavors and essences, and to particles formed from the compositions, and Methods of making and using the compositions. Background technique [0002] Cellulose is a natural polymer. In fact, cellulose is a major component of plant cell walls and the most abundant polysaccharide in nature. Cellulose has been modified in a number of ways in order to achieve different results. Some modifications optimize water solubility, others improve organic solubility, and still others allow cellulose to be used for specific purposes as well, such as as a hemostatic agent, as in the case of oxidized cellulose. [0003] In the pharmaceutical industry, cellulosic materials are often used as binder materials in tablets. Cellulosic materials are also modif...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23G3/00A23G3/42A23G3/50A23G4/00A23G4/10A23G4/20A23L27/00A61K8/02A61K8/73A61Q11/00C08J3/14C08L1/28
CPCA23G4/20C08L1/284A61K8/02C08J2301/00A61Q11/00A61K2800/5422A23L1/2205C08L1/28A23G3/50C08J3/14A23V2002/00A61K8/731A23L1/22016A23G4/10A23G3/42A61K2800/412A23L27/72A23L27/79A23V2200/224A23V2250/51086A23V2250/194
Inventor L·M·波普维尔C·M·布莱恩特L·S·亨森
Owner INTERNATIONAL FLAVORS & FRAGRANCES