High pressure visible micro wave chemical reaction device

A chemical reaction and microwave technology, applied in the field of high-voltage visible microwave chemical reaction device, can solve the problems of high price, low cost, no chemical reaction device, etc., and achieve the effect of wide application range and compact structure

Inactive Publication Date: 2004-12-22
GUANGZHOU INST OF ENERGY CONVERSION - CHINESE ACAD OF SCI
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Problems solved by technology

[0002] Most of the current chemical reaction experiments are water bath heating or electric heating. The power of microwave generators can be continuously adjusted, but they have not been applied to chemical reaction devices.
In addition, microwaves can only completely pass through materials such as glass, ceramics, polytetrafluoroethylene, and polypropylene plastics. It is very expensive to manufacture a reaction device that can withstand high pressure. For pressures greater than 10Mpa, almost only sapphire reactors can be used, and the price is very high. expensive
In recent years, high-pressure resistant quartz glass has been produced in China, and the cost is relatively low, but it has not been introduced into microwave chemical experiments.

Method used

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  • High pressure visible micro wave chemical reaction device
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Embodiment

[0029] figure 1 , figure 2 The high-pressure visible microwave chemical reaction device shown includes a microwave generation / control / transmission system, a chemical reaction kettle, a constant temperature system, and a reaction gas inlet and outlet and metering system;

[0030] Microwave generation / control / transmission system consists of microwave source 4, circulator 3, water load 5, directional coupler 2, three-pin adjuster 1, elbow 15, waveguide 16, square-circle transition 17; microwave source 4 and circulator in the system The other two ends of the circulator 3 are connected to the water load 5 and the directional coupler 2; the directional coupler 2 is connected to the three-pin adapter 1; the three-pin adapter 1 is connected to the elbow 15; the elbow 15 is connected to the waveguide 16 Connection; waveguide 16 is connected with square-circle transition 17; square-circle transition 17 is connected with reactor 9; microwave source frequency is 2.45 GHz, maximum output...

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Abstract

A visual high-pressure microwave heating chemical reactor is composed of microwave generating/controlling/transmitting system, chemical reactor, constant-temp system and reactive gas I/O and metering system. Said chemical reactor consists of stainless steel jacket, protecting stainless steel rings, high pressure resistant glass cylinder, high pressure resistant microwave guide and enclosing head.

Description

technical field [0001] The invention relates to a high-pressure visible microwave chemical reaction device. Background technique [0002] Most of the current chemical reaction experiments are heated by water bath or electric heating. The power of the microwave generator can be continuously adjusted, but it has not been applied to the chemical reaction device. In addition, microwaves can only completely pass through materials such as glass, ceramics, polytetrafluoroethylene, and polypropylene plastics. It is very expensive to manufacture a reaction device that can withstand high pressure. For pressures greater than 10Mpa, almost only sapphire reactors can be used, and the price is very high. expensive. In recent years, high-pressure resistant quartz glass has been produced in China, and the cost is relatively low, but it has not been introduced into microwave chemical experiments. Contents of the invention [0003] The purpose of the present invention is to provide a bran...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J19/12
Inventor 樊栓狮李栋梁梁得青
Owner GUANGZHOU INST OF ENERGY CONVERSION - CHINESE ACAD OF SCI
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