Silicon rubber composition and its preparation process and use
A technology of silicone rubber composition and silicone raw rubber, which is applied in the field of silicone rubber composition and its preparation, can solve problems such as resistance to hydrolysis and unsatisfactory bonding, and achieve the effect of improving bonding strength
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[0018] Example 1
[0019] Prepare silicone rubber in the following proportions:
[0020] 107 Raw Silicone Rubber (Beijing Chemical Plant) 100 parts by weight
[0021] Ethyl orthosilicate (Beijing Xinzhong Chemical Plant) 3 parts by weight
[0022] Dibutyl tin dilaurate (Beijing Chemical Plant) 0.4 parts by weight
[0023] No. 2 white carbon black (Shenyang Chemical Plant) 10 parts by weight
[0024] Titanium dioxide (Beijing Chemical Plant) 40 parts by weight
[0025] γ-(3-acetylacetonyl)propyltrimethoxysilane (homemade) 1 part by weight
[0026] Coated on the surface of 304# stainless steel with a concentration of 1% γ-(3-acetylacetonyl)propyltrimethoxysilane ethanol solution and dried. After being placed at room temperature for 24 hours, the stainless steel test piece was bonded with the silicone rubber. Leave it at room temperature for 7 days to allow the silicone rubber to cure completely. The results of the shear strength test are as follows:
[0027] Shear strength failure m...
Example Embodiment
[0040] Example 2
[0041] Prepare silicone rubber according to the following formula:
[0042] 107 Raw Silicone Rubber (Beijing Chemical Plant) 100 parts by weight
[0043] Ethyl orthosilicate (Beijing Xinzhong Chemical Plant) 3 parts by weight
[0044] Dibutyl tin dilaurate (Beijing Chemical Plant) 0.4 parts by weight
[0045] No. 2 white carbon black (Shenyang Chemical Plant) 10 parts by weight
[0046] Titanium dioxide (Beijing Chemical Plant) 40 parts by weight
[0047] γ-(3-acetylacetonyl)propyltrimethoxysilane (homemade) 1-5 parts by weight
[0048] Bond the brass test piece with the above-mentioned silicone rubber. Place it at room temperature for 24h, and treat it at 100°C for 6h. The results of the shear strength test are as follows:
[0049] γ-(3-acetylacetonyl)propyl tri
[0050] 0 1 3 5
[0051] Methoxysilane content (weight minutes)
[0052] Shear strength (MPa) <0.5 2.46 2.79 2.83
[0053] Failure form Adhesive failure Cohesive failure Co...
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