Producing process for preparing lubricant of papermaking coating with polyvinyl wax oxide as main materials

A technology of oxidized polyethylene wax, the main raw material, applied in the rearrangement of coating materials, etc., can solve the problems of low viscosity, good rheological leveling performance, inability to adapt, and unsatisfactory coating leveling, etc., to achieve infinite The effects of three wastes discharge, easy control and simple process

Active Publication Date: 2005-02-23
HUBEI DAYA BIOLOGICAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This makes the leveling of the coating in the coating process unsatisfactory, so it cannot adapt to the high solid content, low viscosity and rheology of the coating required by the coating process with its technology, equipment level and market requirements for the gloss and smoothness of the finished paper. Good leveling performance requirements

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] 1. Put 1 part of oxidized polyethylene wax and 0.1 part of morpholine into a glass-lined reactor, heat it, and stir it at 115 ° C at a speed of 2500 rpm for 2 hours. During this process, nitrogen gas is introduced to isolate the air, and then Cool down to 80°C, add deionized water with 20% oxidized polyethylene wax, and stir again at 2500 rpm for 2 hours to form a water-in-oil emulsion to form component A;

[0018] 2. Put 1 part of alkylphenol polyoxyethylene ether-10 (OP-10) and 0.2 parts of sodium trimetaphosphate into a glass-lined reactor, heat it, and stir it at 80°C for 5 hours to convert it into an anionic , adjust its pH value to 8-9 by conventional methods, and form component B;

[0019] 3. Put 1 part of silica and 0.2 part of sorbitan monooleate (commonly known as Span-80) into a glass-lined reaction kettle, heat, stir at 180°C at 1200 rpm for 2 hours, then cool down To 80°C, add deionized water with 50% of the amount of silica to form a water mixture emulsio...

Embodiment 2

[0022] 1. Put 1 part of oxidized polyethylene wax and 0.1 part of morpholine into a glass-lined reactor, heat it, and stir it at 2500 rpm for 2 hours at 118 ° C. During this process, nitrogen gas is introduced to isolate the air, and then Cool down to 80°C, add deionized water with 20% oxidized polyethylene wax, and stir again at 2500 rpm for 2 hours to form a water-in-oil emulsion to form component A;

[0023] 2. Put 1 part of octylphenol polyoxyethylene ether-10 (TX-10) and 0.2 parts of sodium trimetaphosphate into a glass-lined reactor, heat it, and stir it at 82°C for 5 hours to convert it into an anion Type, adjust its pH value to 8-9 by conventional methods, and form component B;

[0024] 3. Put 1 part of silica and 0.2 part of sorbitan monooleate (commonly known as Span-80) into a glass-lined reaction kettle, heat, stir at 182°C at a speed of 1200 rpm for 2 hours, and then cool down To 80°C, add deionized water with 50% of the amount of silica to form a water mixture e...

Embodiment 3

[0027] 1. Put 1 part of oxidized polyethylene wax and 0.1 part of morpholine into a glass-lined reactor, heat, stir at 120 °C at a speed of 2500 rpm for 2 hours, pass nitrogen gas during this process to isolate the air, and then Cool down to 80°C, add deionized water with 20% oxidized polyethylene wax, and stir again at 2500 rpm for 2 hours to form a water-in-oil emulsion to form component A;

[0028] 2. Put 1 part of nonylphenol polyoxyethylene ether-10 (NP-10) and 0.2 parts of sodium trimetaphosphate into a glass-lined reactor, heat it, and stir it at 85°C for 5 hours to convert it into an anionic , adjust its pH value to 8-9 by conventional methods, and form component B;

[0029] 3. Put 1 part of silica and 0.2 part of sorbitan monooleate (commonly known as Span-80) into a glass-lined reaction kettle, heat, stir at 185°C at 1200 rpm for 2 hours, then cool down To 80°C, add deionized water with 50% of the amount of silica to form a water mixture emulsion and form C componen...

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PUM

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Abstract

A lubricant with oxidized polyvinyl wax as main material is manufactured by non-ionizing oxidized polyvinyl wax, negative ionizing surfactant OP-10 or TX-10 or NP-10, then composing modified surfactant said above and non-ionized oxidized polyvinyl wax and silicone, emulsifying to prepare solids content 25% products which is oil-in-water type emulsified products. The lubricant is used as special coating for papermaking and has viscosity<30Mpa.s, and its performance/price rate exceeds imported products.

Description

1. Technical field [0001] The present invention relates to manufacturing. A special lubricant for coating, especially the production process of the lubricant prepared from oxidized polyethylene wax as the main raw material. 2. Background technology [0002] When oxidized polyethylene wax is selected as the main raw material to prepare a special lubricant for papermaking coating, its product performance, in terms of stability, smoothness, gloss, surface strength, ink absorption, printing gloss, etc., is superior to that of traditional lubricants. Special lubricants for papermaking coating, for example, paraffin wax emulsion lubricants formed by emulsification after melting paraffin wax as raw materials; water-mixed liquid lubricants formed by stearate (calcium) Lubricant made by addition reaction and gene reaction with organic acid and unsaturated wax as raw material under the action of initiator; and lubricant obtained by emulsification with silicone oil as raw material, al...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21H25/08
Inventor 徐振明
Owner HUBEI DAYA BIOLOGICAL TECH CO LTD
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