Fire resistant cellulosic materials
a cellulosic material and fire-resistant technology, applied in the field of treated cellulosic materials, can solve the problems of fire jumping from house roof to house roof, restrictions on wood use in roofing, etc., and achieve the effect of improving fire-resistant and leach-resistant properties
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example 1
[0046] Example 1 illustrates a first embodiment of this invention
[0047] Wood having an unfinished surface and illustrative of a preferred cellulosic material was soaked in a solution containing aluminum phosphate having an Al.sub.2O.sub.3--P.sub.2O.sub.5 ratio of about 0.33+ / -0.1. The aluminum phosphate solution was heated to a temperature of about 100.degree. C. and the wood was placed in the aluminum phosphate solution of about 10% solids by weight of the total solution for about 20 minutes. A single contact of the phosphate solution was made with the wood. This initially treated wood was removed from the aluminum phosphate solution and allowed to air dry until the surface was dry to the human touch for about one hour, thus, providing an air-dried sample of wood. The air-dried sample of wood was then placed in a microwave oven, which was turned on high power, and irradiated for about 20 seconds to drive out initial water of composition without burning the treated wood and to effec...
example 2
[0048] Example 2 is illustrates a second embodiment of this invention
[0049] Part A: Preparation of Aluminum Phosphate Solution
[0050] Aluminum phosphate solutions were prepared starting with the ratio of Al to P corresponding to chain length of n=100 (Al.sub.2O.sub.3--P.sub-.2O.sub.5 ratio is 1:2.94) with some exceptions for chain length 20 (Al.sub.2O.sub.3--P.sub.2O.sub.5 ratio is 1:2.72). Several metal oxides were added to a hot or boiling aqueous solution of phosphoric acid in such amount to obtain aluminum metal condensed phosphates with chain length n=20. The amounts of metal oxides employed in the phosphate solution were limited by their different solubilities in the phosphate solution. A single solution containing aluminum phosphate was employed in this Example.
[0051] Several samples were made for preliminary testing of metal oxides: ferric / ferrous oxide (3.06% in respect to solid); ferric oxide (2.5%); cupric oxide (1.3%); and zinc oxide (1.23% of mixture 3 parts of zinc oxid...
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Abstract
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