Soot control for diesel engine lubricants
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example 1
[0148]Blends were prepared comprising only GTL 6 of nominal KV 6.0 mm2 / s at 100° C., a mixture of only 150N and 600N Group I base oil the KV of the mixture being nominally 6.0 mm2 / s @ 100° C., and combinations of the GTL 6 and the 150N / 600N base oils. All contained 2.0 wt % (as received) dispersant Infineum C9268. The blends were tested in a soot handling screener test which adds 3 wt % carbon black to the blend replicating 3 wt % soot in the oil.
[0149]The screener test is summarized below:[0150]1. Prepared blend by adding designated amount of carbon black paste (20% carbon black) and test oil to a blender. Blend for 5 minutes at high speed.[0151]2. Transfer mixture to beaker with magnetic stir bar. Stir at 200 rpm for 1 hour at 65° C.[0152]3. Immediately after stirring, charge the mixture to the viscometer in the 100° C. KV bath. Allow sample to equilibrate for exactly 15 minutes, then measure the Kinematic viscosity.[0153]4. For each oil, measure the viscosity increase at each inc...
example 2
[0155]In this Example the relationship between GTL content and the desired thickening ability of two different viscosity modifiers at two different concentrations in blends is investigated. A 6.0 mm2 / s GTL 6 and a 6.0 mm2 / s Group I blend were used. No carbon black was added. The GTL / Group I base stock combinations used in Example 2 are the same as those used in Example 1 above.
TABLE 3% GTL / % Group I Blend0 / 10020 / 8040 / 6060 / 4080 / 20100 / 0Viscosity: Blend with 15 wt16.015.515.214.814.514.2% (as received) Paratone 8011(mm2 / s)Thickening parameter: %1.501.571.641.701.771.82Paratone 8011 / change inKV100Viscosity: Blend with 25 wt15.414.814.213.713.312.9% (as received) InfineumSVs 151 (mm2 / s)Thickening parameter: %2.652.853.053.253.443.64Shellvis 151 / change in KV100
[0156]Larger ratios of % viscosity modifier to change in viscosity represent less thickening ability or solubilizing power of the base stock of the deliberately added viscosity modifier. Smaller values, i.e., lower ratio values are ...
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