Aqueous Suspensions of TMC278
a technology of tmc278 and suspension, which is applied in the field of pharmaceutical compositions, can solve the problems of resistance, no currently available drug therapy is capable of completely eradicating hiv, and emergence of resistant mutants, so as to prevent hiv infection, prevent hiv infection, and prevent the effect of hiv infection
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example 1
Preparation of Nanosuspensions
[0111]Glass bottles of 250 ml and ZrO2 beads, used as the milling media, were sterilized in an autoclave. Five grams of drug substance were put into the 250 ml glass bottle as well as a solution of 1.25 g PLURONIC™ F108 in 60 ml of water for injection. Three hundred grams of ZrO2-beads with an average particle size of 500 μm were added. The bottle was placed on a roller mill. The suspension was micronized at 100 rpm during 72 hours. At the end of the milling process the concentrated nanosuspension was removed with a syringe and filled into vials. The resulting formulation is Formulation 1 in the following table. Determination of the concentration was done by HPLC / UV. A dilution was made to a final concentration of 25 mg / ml of TMC278. The resulting suspension was shielded from light.
[0112]Using similar procedures, Formulations 2, 3 and 4 were prepared. These were titrated with sodium hydroxide 1N solution to a pH of about 7. In formulations 2, 3 and 4 th...
example 2
Kinetic Study
[0113]The present study demonstrates that an injectable formulation of nanonised TMC278 or its HCl-salt results in stable blood plasma levels during a prolonged period of time. This study compares the plasma kinetics of TMC278 base and hydrochloric salt after single intramuscular (IM) or subcutaneous injection of a nanosuspension (Formula 1 of the previous example) at 5 mg / kg in male beagle dogs.
[0114]Six healthy male beagle dogs with body weights ranging from 8 to 16 kg at the start of the study, were used. Each dog was identified by an ear tattoo number. Two dogs were dosed intramuscularly (IM) in the left and right m. biceps femoris (treatment group A). Two dogs were dosed IM with TMC278.HCl (treatment group B). Two dogs were dosed subcutaneously (SC) in the left and right thoracal region. The injection volume was 2×0.1 ml / kg in all treatment groups. A 20 G needle was used.
[0115]Blood samples of 3 ml were taken from the left jugular vein from all dogs on day 0 at 0 h...
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