Analysis of gas samples for determination of physiological states and disease states
a technology of physiological states and gas samples, applied in the field of analysis of gas samples for determination of physiological states and disease states, can solve the problems of difficult early diagnosis of patients, risk to patients, and excessive radiation risk of mammograms, and achieve the effect of saving lives
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example 1
[0095]This example provides a description of methods and system of the present disclosure.
[0096]Materials. Aniline (Sigma >99%) was freshly double distilled before use. Hydrochloric acid HCl (ACS reagent), ammonium persulfate (APS), ammonium hydroxide (25%), chloroform (>99%) and camphor sulfonic acid (CSA) were purchased from Sigma and were used as received. Thin Film film interdigitated platinum film electrodes (IDA) (line spacing 100 μm) were purchased from the Electronic Design Center, Case Western University, precision gas diluter Model 1010 was purchased from Custom Sensor Solutions. A 25 ppm ammonia / dry N2 was used as the calibration standard and was purchased from Prest-O sales.
[0097]Experimental. Polyaniline (PANI) doped with HCl was prepared by chemical oxidative polymerization of aniline in aqueous acidic medium (1M HCl) with APS as an oxidant. It has been reported earlier that higher polymerization yields were obtained by using oxidant to monomer ratio of 1.2. 50 ml of 0...
example 2
[0103]This example provides a description of methods and system of the present disclosure.
[0104]FIGS. 6 through 21 shows data obtained using methods and systems of the present disclosure. The figures described show gas responses on one polyaniline sensor, an example of one sensor with three gases and three sensors on three gases, six sensors on five gases—building the MOLECULAR FRAME, measuring the scent from cancer cells, changing the frame from 5 to four gases, and various other data. See FIG. 8.
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