Cathode active material for lithium secondary battery and lithium secondary battery including the same
a lithium secondary battery and active material technology, applied in the direction of cell components, electrochemical generators, nickel compounds, etc., can solve the problems of degrading the life-span and structural stability of lithium secondary batteries, and not providing sufficient life-span and structural stability
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experimental example 1
[0109](1) Structural Analysis
[0110]SEM Image Analysis
[0111]FIG. 3 is a scanning electron microscope (SEM) image showing a cross-section of a lithium-nickel composite metal oxide particle of Example 13.
[0112]Referring to FIG. 3, the cathode active material for a lithium secondary battery was formed to have a secondary particle structure in which primary particles were aggregated.
[0113]EDS Analysis and XPS Analysis
[0114]FIGS. 4A to 4C are graphs showing results of an energy dispersive X-ray (EDX) analysis at box regions designated as {circle around (1)} to {circle around (3)} in FIG. 3 to measure contents of components in the lithium-nickel composite metal oxide according to an energy.
[0115]Referring to FIGS. 4A to 4C, it can be confirmed that the cathode active material according to exemplary embodiments of the present invention included the lithium-nickel composite metal oxide particle having a transition metal element M1 (Mn, Co) and an element M2 having an oxidation number of +2.
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experimental example 2
[0119](1) Measurement of Initial Resistance and Initial Discharge Capacity
[0120]After charging (CC-CV 0.1 C 4.3V 0.005 C CUT-OFF) the lithium secondary batteries prepared according to Examples and Comparative Examples in a chamber at 25° C., a battery capacity (initial charge capacity) was measured. The batteries were discharged again (CC 0.1 C 3.0V CUT-OFF) and then a battery capacity (initial discharge capacity) was measured.
[0121](2) Measurement of Capacity Retention (Life-Span Property) During Repeated Charging and Discharging
[0122]120 cycles of charging (CC / CV 0.5 C 4.3V 0.05 C CUT-OFF) and discharging (CC 1.0 C 3.0V CUT-OFF) at 45° C. were repeated for the lithium secondary batteries according to Examples and Comparative Examples. A discharge capacity retention was evaluated as a percentage of a value obtained by dividing the discharge capacity at the 120th cycle by the discharge capacity at the first cycle.
[0123]The evaluation results are shown in Table 4 below.
TABLE 4Initial...
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