Microwave method for synthesizing carbonate of natrium glycine

A technology of sodium glycinate and sodium diglycinate is applied in chemical instruments and methods, preparation of organic compounds, organic chemistry and other directions, which can solve the problems of troublesome product separation and purification, low yield, and restrictions on wide application, shortening operation procedures, The effect of shortening the response time and saving energy

Inactive Publication Date: 2008-12-24
SICHUAN UNIV
View PDF3 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the method of producing it is "wet method", that is, it is produced by heating glycine and sodium carbonate in an aq

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0006] 1. Take 7.5 g of glycine and 5.3 g of sodium carbonate, mix thoroughly in a mortar, then place in a glass container, add 7.5 ml of water to make a paste, make it into a "wet-solid phase", and adjust the heating power to 50W, after heating for 20 minutes, stop heating, take out the reaction product after cooling, and pulverize to obtain sodium bisglycinate carbonate product, and the yield can reach about 80%.

[0007] 2. Take 7.5 grams of glycine and 5.3 grams of sodium carbonate, mix thoroughly, add water to make a paste, make it into a "wet-solid phase", then place it in a microwave oven, adjust the heating power to 75W, and heat for 15 minutes. The product is cooled, and then the product is taken out and pulverized to obtain a sodium bisglycinate carbonate product with a yield of over 98%. If the raw material of the reaction product is very pure, the product can be used directly as a food additive and pharmaceutical industry agent without purification.

[0008] 3. Take 3....

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

A microwave method for synthesizing glycine sodium carbonate as the additive of food and medicine is disclosed, which features the microwave 'Wet-solid phase' method instead of 'Wet synthesis'. Its advantages are short reaction time, and high output rate.

Description

Technical field: [0001] The invention relates to a synthesis method of a novel food additive and sodium glycinate carbonate used in the pharmaceutical industry, and belongs to the production field of food additives and pharmaceutical industrial agents. Background technique: [0002] Traditionally used food puffing agent mostly uses NaHCO 3 or NH 4 HCO 3 , or their complex products, which are widely used because of their low price, but they are not satisfactory because of their low solubility or the production of water after reacting with acidic substances in food, which deteriorates the production conditions. In recent years, a class of sodium glycinate carbonate has been developed abroad to replace NaHCO 3 As a puffing agent and an acid regulator, it not only eliminates the shortcomings of the latter, but also glycine itself is needed by the human body, so it is also a nutritional agent, so it has been used abroad. In China, it is mainly used in the pharmaceutical indus...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C07C229/06C07C227/16
Inventor 陈天朗牟元华肖慎修
Owner SICHUAN UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap