Multilayer container
A container and polyethylene layer technology, applied in the field of improvement of multi-layer containers, can solve the problems of reduced bonding strength and impact resistance of polyamide and modified polyethylene layers, etc.
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Embodiment 1
[0042] A resin material for a multilayer structure of a multilayer container was prepared as described below.
[0043] [Polyamide resin mixture]
[0044] In a reactor with stirring blades, 10 kg of ε-caprolactam was stirred at 100° C. until a uniform reaction system was formed. Then, raise the temperature to 260°C, and apply 15kg / cm 2 Stirring was continued under pressure for at least one hour. Next, the pressure was no longer applied, and the reaction was continued for three hours under normal pressure while removing water by volatilization. After the reaction was terminated, the strand-shaped reaction product was collected through the bottom nozzle of the reactor, water-cooled, and cut into polyamide-6 resin pellets with an average molecular weight of 32000.
[0045] After immersing the pellets in hot water and removing unreacted monomers (approximately 10%) by extraction, they were dried in vacuum, resulting in a polyamide resin used as an adhesive layer according to the...
Embodiment 2
[0060]The procedure of Example 1 was repeated except that 5 g of titanium dioxide having an average particle diameter of 15 nm was used instead of 10 g of titanium dioxide having an average particle diameter of 15 nm in Example 1, thereby manufacturing a multilayer container. Table 1 shows the results.
Embodiment 3
[0062] The procedure of Example 1 was repeated except that 10 kg of ε-caprolactam, 0.9 kg of adipic acid and 2 kg of water were used to prepare a polyamide resin mixture, thereby manufacturing a multilayer container. Table 1 shows the results.
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