Radiation sensitive composition for forming a colored layer, color filter and color liquid crystal display device
A technology of sensitivity and composition, applied in the field of color liquid crystal display elements, which can solve the problems of not being able to fully fill the group, etc.
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[0340] Examples are given below to further specifically illustrate the present invention. The present invention is not limited by the following examples. Here, parts and % are based on weight.
[0341] Synthesis of Alkali Soluble Copolymer
Synthetic example 1
[0343] Add 3 parts of 2,2'-azobisisobutyronitrile, 200 parts of propylene glycol monomethyl ether acetate into a flask equipped with a condenser tube and a stirrer, then add 15 parts of methacrylic acid, 25 parts of 3-(methyl Acryloyloxymethyl)-3-ethyloxetane, 60 parts of benzyl methacrylate and 3 parts of α-methylstyrene dimer as a molecular weight regulator, replaced with nitrogen, and then gently Slowly stirring, the temperature of the reaction solution was raised to 80° C., and the temperature was maintained for 5 hours to perform polymerization to obtain a resin solution. This resin was referred to as "alkali-soluble resin (B-1)".
Synthetic example 2
[0345] Add 3 parts of 2,2'-azobisisobutyronitrile, 200 parts of propylene glycol monomethyl ether acetate into a flask equipped with a condenser tube and a stirrer, then add 15 parts of methacrylic acid, 25 parts of 3-(methyl Acryloyloxymethyl)-3-ethyloxetane, 20 parts N-phenylmaleimide, 10 parts styrene, 30 parts benzyl methacrylate and 3 parts as molecular weight regulator The α-methylstyrene dimer was replaced with nitrogen, then gently stirred, the temperature of the reaction solution was raised to 80° C., and the temperature was maintained for 5 hours to perform polymerization to obtain a resin solution. This resin was referred to as "alkali-soluble resin (B-2)".
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