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Refining process of Al-Ti-B intermediate alloy for pure aluminum

A technology of master alloy and pure aluminum, which is applied in the field of refining pure aluminum by using Al-Ti-B master alloy, which can solve the problems of difficult dissolution, difficult dispersion of compound groups, incomplete phase dissolution and diffusion, etc., to improve aluminum materials quality, speed up dissolution and diffusion, and increase nucleation efficiency

Inactive Publication Date: 2008-12-24
BAOSHAN IRON & STEEL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This refinement process can better exert the refinement effect of the Al-Ti-B master alloy, but when the master alloy is added to the aluminum melt, the TiB that was originally agglomerated in a short period of time 2 The compound group is difficult to disperse, its nucleating ability cannot be fully exerted, and in the subsequent rolling processing of aluminum products, the high hardness TiB 2 The agglomeration group is easy to scratch the roll, and there will be perforation and various line defects when rolling aluminum foil; at the same time, the long strip of TiAl 3 The phase is difficult to completely dissolve, so that the solute Ti cannot be uniformly distributed throughout the melt
Therefore, when using this refinement process, due to the coarse TiAl 3 Incomplete phase dissolution and diffusion, adhesion of TiB 2 Particle aggregates cannot be dispersed, so that the refinement efficiency of Al-Ti-B master alloy is very low, and the grain size of industrial pure aluminum as-cast after refinement by this process is generally greater than 150 μm

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] Weigh industrial pure aluminum and melt it, heat up to 700°C and keep it warm for 15 minutes, add the Al-5Ti-1B master alloy weighed by 0.3% of the weight of industrial pure aluminum into the industrial pure aluminum melt at 700°C, and then The upper part of the body is introduced with a frequency of 20KHz, a high-energy ultrasonic wave with a power of 3000W, and the ultrasonic vibration treatment is continued for 3 minutes.

Embodiment 2

[0016] The embodiment is the same as that in Example 1, wherein the temperature of the aluminum melt is 730° C., the addition amount of Al-5Ti-1B is 0.2%, the frequency of the high-energy ultrasonic wave is 21KHz, the power is 2000W, and the continuous treatment time is 2 minutes.

Embodiment 3

[0018] The embodiment is the same as that of Example 1, wherein the temperature of the aluminum melt is 760° C., the addition amount of Al-5Ti-1B is 0.5%, the frequency of the high-energy ultrasonic wave is 19KHz, the power is 5000W, and the continuous treatment time is 5 minutes.

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PUM

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Abstract

The invention provides a process of Al-Ti-B master alloy on grain refinement of pure aluminum. In the invention, except for the addition of the Al-Ti-B master alloy grain refiner in the aluminum melt, the high energy ultrasonic vibration treatment is also adopted, thereby speeding up dissolving and dispersing of TiAl3 phase, increasing the dispersive distribution degree of TiB2 grains and further improving the grain refinement efficiency of the Al-Ti-B master alloy. Industrial pure aluminum as-cast crystal grains treated by the grain refinement process of the invention are all fine isometric crystals, the average size of which is less than 150 mu m, thereby not only improving the quality of aluminum materials but also meeting the requirements on the subsequent rolling of aluminum products.

Description

technical field [0001] The invention relates to the technical field of metal material processing, in particular, the invention relates to a process for refining pure aluminum by using an Al-Ti-B master alloy. Background technique [0002] Grain refinement is one of the important means to improve the strength and plasticity of materials, and is an important way to improve the quality of aluminum materials. With the widespread use of aluminum materials, especially in high-tech fields, the subsequent deep processing of aluminum ingots and The structure in the process puts forward strict requirements, and the key to controlling its structure and performance is to cast the best as-cast grain structure. Grain size and morphology are important characteristics of the as-cast structure, and fine and uniform equiaxed grains are the best as-cast structure. To obtain this structure, the grains must be refined by different means. The means to refine the as-cast structure of metals and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/03B22D21/04B22D27/20
Inventor 张立方园
Owner BAOSHAN IRON & STEEL CO LTD
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