Pressure sensitive adhesive tape
A pressure-sensitive adhesive and pressure-sensitive adhesive layer technology, applied in the field of pressure-sensitive adhesive tapes, can solve the problems of improved rewinding ability, reduced adhesive strength, and practical problems of tapes
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preparation Embodiment 1
[0126]To 100 parts by weight of a mixture containing 70 wt.% n-butyl acrylate, 29.5 wt.% 2-ethylhexyl acrylate and 0.5 wt.% methacrylic acid, add 0.03 parts by weight of a water-soluble azo-type as a polymerization initiator Initiator (commercial product V-50 of Wako Pure Chemical Industries), emulsified with 2 parts by weight of reactive emulsifier (commercial product Aqualon BC-2020 of Daiichi Kogyo Seiyaku), and then passed at about 60° C. to polymerize by mixing Mode of emulsion polymerization Polymerization was carried out for 2 hours to obtain an emulsion of an acrylic polymer (which may be referred to as "acrylic emulsion polymer A"). In this acrylic emulsion polymer A, the emulsion particles had an average particle size of 0.128 μm.
preparation Embodiment 2
[0128] To 100 parts by weight of a mixture containing 70 wt.% n-butyl acrylate, 28.75 wt.% 2-ethylhexyl acrylate and 1.25 wt.% methacrylic acid, add 0.1 parts by weight of a water-soluble azo-type as a polymerization initiator Initiator (commercial product V-50 of Wako Pure Chemical Industries), and emulsify it with 2 parts by weight of reactive emulsifier (commercial product Aqualon BC-2020 of Daiichi Kogyo Seiyaku), and then pass through at about 60° C. to continuously drop Emulsion Polymerization in Polymerization Mode Polymerization was performed for 2 hours to obtain an emulsion of an acrylic polymer (which may be referred to as "acrylic emulsion polymer B"). In this acrylic emulsion polymer B, the emulsion particles had an average particle size of 0.141 μm. In the aqueous system (aqueous phase) to which the emulsion containing the monomer component is added dropwise, pre-add the mixture containing n-butyl acrylate, 2-ethylhexyl acrylate and methacrylic acid relative to 1...
preparation Embodiment 3
[0130] To 100 parts by weight of a mixture comprising 70 wt.% n-butyl acrylate, 28.75 wt.% 2-ethylhexyl acrylate and 1.25 wt.% methacrylic acid, add 0.005 parts by weight of a silane coupling agent (Shin-etsu Silicone commercial product KBM-503) and 0.1 parts by weight of a water-soluble azo-type initiator (commercial product V-50 of Wako Pure Chemical Industries) as a polymerization initiator, and 2 parts by weight of a reactive emulsifier (commercial product Aqualon of Daiichi Kogyo Seiyaku BC-2020) was emulsified, and then polymerized at about 60° C. for 2 hours to obtain an emulsion of an acrylic polymer (which may be referred to as “acrylic emulsion polymer C”). In this acrylic emulsion polymer C, the emulsion particles had an average particle size of 0.158 μm. In the aqueous system (aqueous phase) to which the emulsion containing the monomer component is added dropwise, pre-add the mixture containing n-butyl acrylate, 2-ethylhexyl acrylate and methacrylic acid relative t...
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