Volume hologram optical recording medium, composition for volume hologram recording layer formation, and volume hologram recording material
A technology of optical recording medium and volume holography, which is applied in the direction of photosensitive materials, optics, and optomechanical equipment used in optomechanical equipment. /N ratio and excellent reliability
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Embodiment 1
[0243] Weigh 7.892g of the compound added with 2-ethylhexanol in the hexamethylene diisocyanate polymer, p-cumylphenol EO modified Acrylate 1.667g, (η5-2,4-cyclopentadiene-1-yl)-bis(2,6-difluoro-3-(1H-pyrrole-1-yl)-phenyl)titanium 0.083 g. Put 0.0083 g of terpinolene into sample bottle 1, and stir until each component is dissolved.
[0244] Next, 7.108 g of polycaprolactone triol with a molecular weight of 500 and 0.003 g of dioctyltin dilaurate were weighed into sample bottle 2, and stirred until each component was dissolved.
[0245] Then, the sample bottles 1 and 2 were put into a bell-shaped sintering furnace, and after 3 hours of vacuum degassing, the liquids in the sample bottles 1 and 2 were mixed together and stirred to mix, and the bell-shaped sintering furnace was vacuum-degassed for several minutes.
[0246] Next, on an aluminum-deposited glass plate (on the side on which the aluminum is deposited) provided with Teflon (registered trademark) sheets with a thicknes...
Embodiment 2
[0248] Same as Example 1, weigh hexamethylene diisocyanate 4.743g, tribromophenyl acrylate 1.667g, bis(η 5-2,4-cyclopentadiene-1-yl)-bis(2,6 0.083 g of -difluoro-3-(1H-pyrrole-1-yl)-phenyl)titanium and 0.0083 g of terpinolene were put into sample bottle 1, and stirred until each component was dissolved.
[0249] Also, 10.257 g of polycaprolactone triol with a molecular weight of 500 and 0.003 g of dioctyltin dilaurate were weighed into sample bottle 2, and stirred until each component was dissolved.
[0250] Then, the same operation as in Example 1 was performed to prepare a recording layer.
Embodiment 3
[0252] Same as Example 1, weigh 7.892g of the compound added with 2-ethylhexanol in the hexamethylene diisocyanate polymer, 1.667g of tribromophenyl acrylate, bis(η5-2,4-cyclo Pentadiene-1-yl)-bis(2,6-difluoro-3-(1H-pyrrole-1-yl)-phenyl)titanium 0.083g, γ-terpinene 0.0083g into the sample bottle 1, stir until all ingredients are dissolved.
[0253] Also, 7.108 g of polycaprolactone triol with a molecular weight of 500 and 0.003 g of dioctyltin dilaurate were weighed into sample bottle 2, and stirred until each component was dissolved.
[0254] Then, the same operation as in Example 1 was performed to prepare a recording layer.
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