Intumescent flame retardant (IFR) material containing metal oxygenation substances and preparation method thereof
An intumescent flame retardant and oxygen compound technology, applied in the field of flame retardant polymers, can solve the problems of product performance deterioration, poor flame retardant effect, large addition amount, etc., achieve low production cost, good flame retardant effect, and improve flame retardant efficiency effect
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Embodiment 1
[0014] Example 1 Intumescent flame retardant material containing metal oxygenate and its preparation method, each component is proportioned according to the following weight percentage:
[0015] Resin matrix 70℅,
[0017] Melamine Pyrophosphate 20℅,
[0018] Pentaerythritol 7℅;
[0019] Add 1.5% of resin weight curing agent to the above mixture, add 6% of resin weight anti-shrinkage agent, add 2% of mixture weight thickener, add 1% of mixture weight internal release agent, 30-50 ℃ Knead evenly, knead during kneading, then crush the kneaded premix, extrude and granulate through an extruder, and then injection mold through an injection molding machine. The combustion phenomenon detected by the experiment in this embodiment shows that there is no droplet, the carbon layer expands obviously, and there is no collapse; its oxygen index (LOI) / % is 29.0. According to the test results, only adding IFR(2 # ) The limiting oxygen index (LOI) of the base materi...
Embodiment 2
[0020] Example 2 Intumescent flame retardant material containing metal oxygenate and its preparation method, each component is proportioned according to the following weight percentages:
[0021] Resin matrix 70℅,
[0022] Aluminum Oxide 5℅,
[0023] Melamine Pyrophosphate 18℅,
[0024] Pentaerythritol 7℅;
[0025] The preparation method is to knead the above-mentioned components with good ratio in kneading, then break the kneaded premix, extrude and granulate through an extruder, and then shape it by hot pressing. The experimental detection of this embodiment shows that there is no molten droplet and the charcoal layer is dense; its oxygen index (LOI) / % is 29.4. According to the test results, only adding IFR(2 # ) The limiting oxygen index (LOI) of the substrate of the flame retardant system is 25.0%.
Embodiment 3
[0026] Example 3 Intumescent flame retardant material containing metal oxygenate and its preparation method, each component is proportioned according to the following weight percentage:
[0027] Resin matrix 70℅,
[0028] Zeolite 5℅,
[0029] Melamine Pyrophosphate 18℅,
[0030] Pentaerythritol 7℅;
[0031] The preparation method is to knead the above-mentioned well-proportioned components in kneading, then crush the kneaded premix, extrude and granulate through an extruder, and then injection molding or hot-press molding by an injection molding machine. The experimental detection of this embodiment shows that there is no molten droplet, and the charcoal layer is dense and firm; its oxygen index (LOI) / % is 29.6. According to the test results, only adding IFR(2 # ) The limiting oxygen index (LOI) of the substrate of the flame retardant system is 25.0%.
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