Low-temperature co-fired ceramic medium material and preparation method thereof

A low-temperature co-fired ceramic and dielectric material technology is applied in the field of ceramic dielectric materials and their preparation, and can solve the problems of high loss, low dielectric constant, and narrow range of adjustable sintering shrinkage.

Inactive Publication Date: 2010-09-08
TIANJIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At present, more low-temperature sintered ceramic materials are reported to be BaTi 4 o 9 Department, Li 2 O-Nb 2 o 5 -TiO 2 Department, ZnNb 2 o 6 system and ZnTiO 3 However, these low-temperature sintered ceramic materials have problems such as low dielectric constant, high loss and narrow range of adjustable sintering shrinkage.

Method used

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  • Low-temperature co-fired ceramic medium material and preparation method thereof
  • Low-temperature co-fired ceramic medium material and preparation method thereof
  • Low-temperature co-fired ceramic medium material and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment

[0018] Example Large Group 1

[0019] Raw material BaTiO 3 、 Bi 2 o 3 、Nd 2 o 3 and TiO 2 According to the formula Ba 6-3x (Nd 0.4 Bi 0.6 ) 8+2x Ti 18 o 54 , where x=0.8, batching, ball milling on a ball mill with a rotating speed of 400r / min for 6 hours, drying at 100°C in a 3.3kw ordinary oven, passing through 250 holes / cm 2 Sieve the sample, raise the temperature to 980°C at 5°C / min, and keep it at 980°C for 3 hours to obtain frit A. According to the proportions stated in the table below, the molten water is cooled, ground, and sieved to obtain glass powder B and glass powder C

[0020] Element

Li 2 CO 3 (g)

SiO 2 (g)

h 3 BO 3 (g)

LiF(g)

BaF 2 (g)

total

Glass Powder B

40

10

50

0

0

100

Glass Powder C

0

0

0

20

80

100

[0021] Carry out secondary batching, ball mill on a ball mill at a speed of 400r / min for 8 hours, dry at 120°C, pass throu...

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Abstract

The invention discloses a low-temperature co-fired ceramic medium material. The material consists of 1 to 16 weight percent of glass powder and 84 to 99 weight percent of Ba6-3x(Nd0.4Bi0.6)8+2xTi18O54, wherein the x is 0.5 to 1.5. The glass powder is at least one of the following two types of glass powder, namely glass powder B consisting of 30 to 50 mass percent of Li2CO3 and 5 to 20 mass percent of SiO2 and 40 to 60 mass percent of H3BO3 and glass powder C consisting of 15 to 40 mass percent of LiF and 60 to 85 mass percent of BaF2. In a preparation process, first, clinker is prepared; then, secondary preparation of the glass powder and the clinker is performed; and finally, sintering is performed. A BaO-Nd2O3-Bi2O3-TiO2 system is selected and a method of adding the glass powder as a sintering aid is adopted, so the material has the characteristics of sintering temperature below 900 DEG C, high dielectric constant and low dielectric loss, simultaneously has a wide sintering shrinkage range, and can be co-fired with a silver metallic electrode with high conductivity.

Description

technical field [0001] The invention relates to a ceramic dielectric material and a preparation method thereof, more specifically, to a low-temperature co-fired ceramic dielectric material and a preparation method thereof. Background technique [0002] The development of information technology requires high-speed data and high current density transmission, and electronic circuits are increasingly developing in the direction of miniaturization, integration and high frequency. This puts forward requirements for electronic components with small size, high frequency, high reliability, low price and high Integration requirements. In recent years, low-temperature co-fired ceramics (LTCC) technology has brought great flexibility to the design of multilayer circuits and electronic components, and has become a research hotspot. [0003] Since this technology requires different dielectric materials (such as capacitors, substrates, etc.), magnetic dielectric materials (such as inducto...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/475C04B35/622
Inventor 吴顺华张永刚高顺起魏雪松陈志斌
Owner TIANJIN UNIV
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