Continuous production technique for ethoxyl ethylene diamine and reaction kettle thereof

A technology of hydroxyethylethylenediamine and production process, which is applied in the production technology field of continuous production of hydroxyethylethylenediamine, can solve the problems of high energy consumption, large circulation amount of by-reaction product raw materials, and high liquid-gas molecular ratio. , to achieve the effect of reducing energy consumption and by-products, the production process is simple and convenient, and easy to operate

Inactive Publication Date: 2010-09-15
苏州联胜化学有限公司
View PDF0 Cites 5 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0014] Another purpose of this patent is to realize the instantaneous reaction of gas and liquid two phases, and at the same time achieve the purpose of controlling side reactions, a new type of practical instantaneous reaction device, to solve the problem of high side reaction products in traditional kettle reactors and other reactors. There are disadvantages of large raw material circulation (high liquid-gas molecular ratio) and high energy consumption; the continuous production of hydroxyethyl ethylenediamine is realized, which ensures the safety of production and the stability of product quality

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Continuous production technique for ethoxyl ethylene diamine and reaction kettle thereof
  • Continuous production technique for ethoxyl ethylene diamine and reaction kettle thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0049] 1 is the top decondenser, 2 is the stripping section of the rectification reaction tower, 3 is the ring ethyl buffer tank, 4 is the reboiler of the tower kettle, 5 is the rectification section of the rectification reaction tower, and 15 is the reaction of the rectification reaction tower 5 is the first inlet, 6 is the second inlet, 7 is the first central tube, 8 is the second central tube, 9 is the gas collection ring, 10 is the liquid collection ring, 11 is the air outlet, 12 is the reaction liquid outlet , 13 is a tear hole, 14 is a ring B uniform distribution hole, 15 is a reactor, and 16 is a round copper fixed distance.

[0050] The raw material ethylenediamine 600KG (99%) is poured into the high-level metering tank, and enters the ethylenediamine heater to be heated to 110°C through the potential difference gravity flow (not shown in the figure), and the flow rate is controlled by the flow meter to 1200L / H, along the first inlet 5 enters the first central pipe 7 a...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses a continuous production technique for ethoxyl ethylene diamine, which comprises the following steps: the raw material ethylene diamine is thrown into a high order metering tank so that the ethylene diamine naturally flows into an ethylene diamine heater through level difference, the ethylene diamine is heated to 100-120 DEG C, and the ethylene diamine enters a reactor after controlling the flow rate to 1000-1600 L / H by a flowmeter; the raw material oxirane enters the reactor after controlling the flow rate to 10-30 L / H by an oxirane storage tank; and the raw materials react in the reactor to generate the reactant liquor. The invention also discloses a reactor for continuous production of ethoxyl ethylene diamine. The technique realizes continuous production of ethoxyl ethylene diamine, has the advantages of simple and convenient production technique, and easy operation, and ensures production safety and stable product quality.

Description

technical field [0001] The invention relates to a production process for continuous production of hydroxyethylethylenediamine and a reaction device for continuous production of hydroxyethylethylenediamine. Background technique [0002] The kettle reactor is a reactor widely used in production. It can be used for homogeneous reactions, and can also be used for heterogeneous reactions dominated by liquid phases. The structure of the tank reactor is mainly composed of four parts: the shell, the stirring device, the shaft seal and the heat exchange device. The shell structure of the kettle reactor includes a cylinder, a bottom, a cover (or a head), a hand hole or a manhole, a sight glass and various process nozzles, etc. The kettle-type reactor in the prior art is mainly used in the instant reaction process of the gas and liquid two phases in the chemical reaction engineering, realizes the full contact of the gas and the liquid two phases and generates a reaction product in a ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C07C215/14C07C213/04
Inventor 蒋全良李学民
Owner 苏州联胜化学有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap