Oil displacement agent
An oil-displacing agent and surfactant technology, applied in the field of oil-displacing surfactants, can solve the problems of chromatographic separation, unsatisfactory use effect, and restricting the development of surfactants.
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[0018] Synthesis of N,N'-Dilauroylethylenediamine Sodium Dipropionate.
[0019] 1. Synthetic intermediates
[0020] In the three-necked flask, add an appropriate amount of anhydrous ethylenediamine, heat it in a water bath to about 50°C, and slowly add methyl acrylate dropwise, wherein ethylenediamine:methyl acrylate=1:2 in terms of moles, and continue stirring after the dropwise addition After 3-4 hours of reaction, unreacted substances were distilled off to obtain intermediates.
[0021] 2. Synthetic secondary products
[0022] In the four-necked flask, add a certain amount of intermediate, dissolve it in a certain amount of acetone, use diethylamine to control the system pH=9-10, and add lauroyl chloride and anhydrous triethylamine dropwise under stirring, wherein Intermediate in terms of moles: lauroyl chloride = 1: 2. Continue to react for 6 hours after the dropwise addition. After the reaction, remove the solvent acetone and the generated triethylamine hydrochloride to...
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