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Al-Zn-Mg-Cu aluminum alloy deformation-solid solution heat treatment technology

A solution heat treatment, aluminum alloy technology, applied in the field of deformation heat treatment of metal materials, deformation heat treatment process, can solve the problems of intensified recrystallization, unfavorable alloy strength, plasticity and fracture toughness, etc., to achieve convenient operation, plasticity and fracture toughness improvement , The effect of simple process method

Active Publication Date: 2011-11-16
湖南中创空天新材料股份有限公司
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  • Claims
  • Application Information

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Problems solved by technology

In addition, in the conventional solution heat treatment process of Al-Zn-Mg-Cu ultra-high-strength aluminum alloy, there is a contradiction between the solid solution crystal phase and the inhibition of recrystallization, that is, to increase the solution temperature or prolong the solution time to completely dissolve Crystalline phase, but intensifies recrystallization, which is not conducive to the improvement of alloy strength, plasticity and fracture toughness

Method used

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  • Al-Zn-Mg-Cu aluminum alloy deformation-solid solution heat treatment technology
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  • Al-Zn-Mg-Cu aluminum alloy deformation-solid solution heat treatment technology

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Embodiment 1

[0025] Embodiment 1-11 adopts the homogenized Al-7.5Zn-1.6Mg-1.5Cu-0.13Zr (mass fraction) aluminum alloy cast slab, adopts as attached figure 1 Deformation-solution heat treatment is carried out in the process flow shown, and the deformation amount, pre-solution and short-term re-solution conditions are specifically shown in Examples 1-11, and the aging treatment is carried out through a two-stage aging system (110°C / 6h+160°C / 10h ); Embodiment 12 adopts Al-6.5Zn-2.4Mg-2.2Cu-0.15Zr according to attached figure 1 The shown technological process carries out deformation, solution heat treatment, and deformation, solution and aging process are the same as embodiment 1; Embodiment 13 adopts Al-5.6Zn-2.5Mg-1.6Cu-0.23Cr, according to the attached figure 1 Deformation and solution heat treatment are carried out in the process flow shown, and the deformation, solution and aging processes are the same as in Example 1; the chemical composition of the alloy in Comparative Example 1 is the ...

Embodiment 2

[0030] The sample was pre-deformed by 10% at 400°C; then pre-solutionized at 440°C for 30 minutes; then deformed by 60% at 400°C; water-quenched at 470°C for 10 minutes; and finally double-stage aging.

Embodiment 3

[0032] The sample was pre-deformed by 95% at 400°C; then pre-solutionized at 440°C for 30 minutes; re-deformed by 60% at 400°C; water-quenched at 470°C for 10 minutes; and finally double-stage aging.

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Abstract

The invention relates to an Al-Zn-Mg-Cu aluminum alloy deformation-solid solution heat treatment technology, which comprises the following steps: (1) pre-deformation, wherein the temperature range of pre-deformation is 400 DEG C - 420 DEG C, the deflection amount is 10% - 95%; (2) pre-solid solution, wherein the temperature range of pre-solid solution is 440 DEG C - 480 DEG C, the insulation timeis 30 - 120 minutes; (3) re-deformation, wherein the temperature range of pre-deformation is 400 DEG C - 420 DEG C, the deflection amount is 10% - 95%; (4) solid solution for short time, wherein the temperature range of solid solution is 470 DEG C - 485 DEG C, the solid solution time is 10 - 30 minutes. According to the invention, the deformation and solid solution are carried out alternatively,which avoids the problem that high dislocation concentration generated in the deformation process of single deformation-solid solution leads to the recrystallization of a substrate; the temperature of the pre-solid solution is higher than the general annealing temperature, the pre-solid solution process after pre-deforming reduces the dislocation concentration introduced by deformation through replying and performs a solid solution to most crystallization phases; the pre-solid solution for short time is performed again for dissolving the residual crystallization phases and inhibiting the crystallization of alloys. The invention has the advantages of simple process and convenient operation, and effectively reduces crystallization phases and re-crystallization of the Al-Zn-Mg-Cu system superhigh strength aluminum alloy, the alloy strength, plasticity and fracture toughness of the alloy after quenching and aging are substantially raised; the technology provided in the invention has significance to the development of the aerospace and traffic transportation fields, and is suitable for an industrial application.

Description

technical field [0001] The invention relates to a deformation heat treatment process for improving the strength, plasticity and fracture toughness of an ultra-high-strength aluminum alloy, in particular to a deformation-solution heat treatment process for an Al-Zn-Mg-Cu series aluminum alloy. The invention belongs to the technical field of metal material deformation heat treatment technology. Background technique [0002] Al-Zn-Mg-Cu ultra-high-strength aluminum alloys are an important class of lightweight and high-strength structural materials, which are widely used in aerospace, transportation and other fields. Al-Zn-Mg-Cu ultra-high-strength aluminum alloys usually adopt a single deformation-solution heat treatment process or multiple deformation-intermediate annealing treatment (the annealing temperature is generally 400-420 ° C), and finally a solution treatment to improve its Comprehensive mechanical properties; conventional single deformation-solution process after i...

Claims

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Application Information

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IPC IPC(8): C22F1/053
Inventor 陈康华陈送义彭国胜
Owner 湖南中创空天新材料股份有限公司
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