Preparation method for litchi pericarp extract and application of same in production of cigarette
A technology of lychee peel and extract is applied in the field of preparation of lychee peel extract to achieve the effects of reducing thorns, removing impurities and releasing amount, improving the comprehensive quality of cigarettes, and improving compatibility.
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Embodiment 1
[0030] (1) Put the fresh lychee peel into an oven at 40°C, bake it with hot air for 12 hours, take it out and cool it naturally, then crush it, and pass through a 60-mesh sieve to get the lychee peel powder;
[0031] (2) according to the mass ratio of litchi peel powder and sherwood oil is the ratio of 1: 3, reflux leaching litchi peel powder with sherwood oil, the temperature of reflux leaching is 40 ℃; Extraction time is 1 hour; Collect after reflux leaching solid residue;
[0032] (3) Add water to the solid residue described in step (2), add hemicellulase for enzymolysis; the mass ratio of the solid residue to water is 1:3; the amount of the hemicellulase is based on the solid Determined by 0.1% of the residue mass; use dilute H 3 PO 4 (The concentration is not strictly limited) Adjust the pH value of the system to 4, the enzymolysis temperature is 40°C, and the enzymolysis time is 2 hours;
[0033] (4) Add absolute ethanol to the enzymolysis solution prepared in step (3...
Embodiment 2
[0037] (1) Put the fresh lychee peel into an oven at 40°C, bake it with hot air for 12 hours, take it out and cool it naturally, then crush it, and pass through a 100-mesh sieve to get the lychee peel powder;
[0038] (2) according to the mass ratio of litchi peel powder and sherwood oil is the ratio of 1: 3, reflux leaching litchi peel powder with sherwood oil, the temperature of reflux leaching is 40 ℃; Extraction time is 1 hour; Collect after reflux leaching solid residue;
[0039] (3) Add water to the solid residue described in step (2), add hemicellulase for enzymolysis; the mass ratio of the solid residue to water is 1:4; the amount of the hemicellulase is based on the solid Determined by 0.5% of the residue mass; with H 3 PO 4 The pH value of the system was adjusted to 5, the enzymolysis temperature was 40°C, and the enzymolysis time was 4 hours;
[0040] (4) Add absolute ethanol to the enzymolysis solution prepared in step (3), the volume ratio of the absolute ethan...
Embodiment 3
[0044] (1) Put the fresh lychee peel into a 60°C oven, bake it with hot air for 5 hours, take it out and cool it naturally, crush it and pass it through a 120-mesh sieve to get the lychee peel powder;
[0045] (2) according to the mass ratio of litchi peel powder and sherwood oil is the ratio of 1: 5, reflux leaching litchi peel powder with sherwood oil, the temperature of reflux leaching is 60 ℃; Extraction time is 2 hours; Collect after reflux leaching solid residue;
[0046] (3) Add water to the solid residue described in step (2), add hemicellulase for enzymolysis; the mass ratio of the solid residue and water is 1:5; the amount of the hemicellulase is according to the residue quality 1% is determined; the enzymatic hydrolysis temperature is 60°C, and the pH value of the system is determined by H 3 PO 4 Adjust to 6, enzymatic hydrolysis time to 6 hours;
[0047] (4) Add absolute ethanol to the enzymolysis solution prepared in step (3), the volume ratio of the absolute e...
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