Enzyme-linked immunoassay detection reagent kit for human insulin-like growth factor II
A technology of enzyme-linked immunoassay and detection kit, which is applied in the direction of biological testing, material inspection products, etc., can solve the problems of high price, pollution and radiation, and achieve the effect of sensitive detection
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0015] Example 1 Preparation of Human Insulin-like Growth Factor II ELISA Detection Kit
[0016] 1. Materials
[0017] Three big-eared white rabbits for immunization, male, weighing 1.5 kg, were provided by the Animal Experiment Center of 301 Hospital. Human IGF Ⅱ polypeptide was purchased from Beijing Boaosen Biotechnology Co., Ltd., and human insulin-like growth factor Ⅱ standard product was purchased from sigma company.
[0018] 2. Preparation and purification of human insulin-like growth factor II antibody
[0019] IGFⅡ and thyroglobulin (TG) were fed according to the optimal molecular ratio (1:100), connected by glutaraldehyde method, subpackaged after dialysis, and freeze-dried to prepare IGFⅡ-TG.
[0020] For the first immunization, IGFⅡ-TG 200 μg and Freund’s complete adjuvant 4ml were fully mixed, and injected into the back of 3 rabbits at multiple points, and boosted immunization once every 4 weeks (100 μg of immunogen and Freund’s incomplete adjuvant 4ml Mix well...
Embodiment 2
[0028] Embodiment 2 detection method
[0029] 1. Preparation of solid-phase antibody microtiter plate
[0030] Take the purified IGFⅡ antibody, prepare 10ug / ml with 0.05M citrate buffer, add 200μl per well into 96-well ELISA plate, incubate at 37°C for 3h, wash the plate, add 3% bovine serum Put albumin in Tris.HCl blocking solution overnight at 4°C, shake off the blocking solution, use a freeze dryer to remove excess water in the well, put it into a tin foil bag and vacuum seal it with a vacuum packaging machine, and store at 4°C.
[0031] 2. Preparation of reagents and instruments
[0032] 1 bottle of freeze-dried human insulin-like growth factor Ⅱ standard substance: each bottle is dissolved in 0.5mL of experimental buffer and the concentration is 250, 83, 27, 9, 3, 1 ng / mL; biotinylated human insulin-like growth factor Ⅱ 1 bottle; 1 bottle of avidin-labeled horseradish peroxidase working solution; chromogenic reagent A: 1 bottle; chromogenic reagent B: 1 bottle, chromoge...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More 