Donkey-hide gelatine raw powder and preparation method thereof
A collagen powder and collagen technology, which can be used in pharmaceutical formulations, powder delivery, unknown raw materials, etc., can solve the problems of easy moisture absorption, unfavorable preservation, and moisture absorption of powdered donkey-hide gelatin.
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experiment example 1
[0026] Experimental Example 1 Comparison of the solubility of donkey-hide gelatin powder, donkey-hide gelatin granules, donkey-hide gelatin blocks, donkey-hide gelatin directly crushed granules, and donkey-hide gelatin spray-dried powder
[0027] Donkey-hide gelatin powder is prepared by the method of Example 4 of the present invention; donkey-hide gelatin granules, donkey-hide gelatin blocks, donkey-hide gelatin directly pulverized particles and donkey-hide gelatin spray-dried powder are all provided by Shandong Dong'e-hide gelatin Co., Ltd.
[0028] (1) Take respectively 20 grams of donkey-hide gelatin powder, donkey-hide gelatin granules, donkey-hide gelatin blocks, donkey-hide gelatin directly pulverized powder, and donkey-hide gelatin spray-dried powder;
[0029] (2) Add 400ml of water, then stir with a glass rod for 3 minutes;
[0030] (3) According to the solubility, only the donkey-hide gelatin powder of the present invention is completely dissolved, and all the other ...
experiment example 2
[0032] Experimental example 2 Density screening of donkey-hide gelatin solution obtained before vacuum drying and powder making of the present invention
[0033] (1) Prepare solutions A and B according to the method described in Example 4 of the present invention, mix solutions A and B, concentrate to a temperature of 15-30° C., and relative densities of 1.10, 1.12, 1.15, 1.20 and 1.26, respectively Donkey-hide gelatin solution, the donkey-hide gelatin solution of above-mentioned density is carried out vacuum continuous drying experiment under the process parameter described in embodiment 4 respectively;
[0034] (2) Experimental results have confirmed that the donkey-hide gelatin powder prepared by the donkey-hide gelatin solution with a relative density of 1.15 and 1.20 has the best solubility and can be completely dissolved in the same time, while the donkey-hide gelatin powder prepared by a donkey-hide gelatin solution with a density lower than 1.15 and higher than 1.20 Po...
experiment example 3
[0036] Time data screening of experimental example 3 vacuum continuous drying
[0037] In view of the fact that the conveyer belt of the vacuum continuous drying equipment is carried out at a uniform speed, at the same temperature, five time gradients were designed for experiments, which were 10 minutes, 15 minutes, 20 minutes, 25 minutes and 30 minutes, and the results confirmed that the collagen dried for 15 minutes The powder is relatively ideal in terms of color, appearance, shape, and solubility. The drying time determined by the drying test is 15 minutes per section.
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