Lithium-ion secondary battery and anode pole piece thereof
A positive pole piece and secondary battery technology, applied in secondary batteries, battery electrodes, circuits, etc., can solve the safety problems of lithium-ion secondary batteries, affect the charging performance of batteries, and deteriorate the low-temperature performance of batteries. Improved thermal safety, good safety performance, and the effect of preventing further rise in temperature
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Embodiment 1
[0031] Preparation of the positive electrode active material: lithium manganese phosphate (LiMnPO 4 , the average particle size is 100nm) is the active material of the core layer, BaTiLa 0.1 o 3 (the average particle diameter is 10nm) is the shell active material, and the positive electrode active material with the core-shell structure is prepared. Firstly, 1 part by weight of BaTiLa 0.1 o 3 with 99 parts by weight of LiMnPO 4Mix, then process at 2500 rpm for 4 minutes, and finally process at 450° C. for 5 hours, so as to prepare a positive electrode active material with a core-shell structure.
[0032] Preparation of the positive electrode sheet: the above-mentioned positive electrode active material with a core-shell structure is used as the active material, and its weight content (relative to the weight of the powder, the same below) is 90%; polyvinylidene fluoride (PVDF) is used as the binder , and its weight content is 5%; with carbon black as the conductive agent, i...
Embodiment 2
[0038] Different from Example 1 is the preparation of the positive electrode active material:
[0039] Lithium manganese phosphate (LiMnPO 4 , with an average particle size of 1000nm) is the active material of the core layer, BaTiSr 0.1 o 3 (average particle size of 1nm) and conductive carbon as shell active material (conductive carbon and BaTiSr 0.1 o 3 The mass ratio is 2:98) to prepare a positive electrode active material with a core-shell structure. Firstly, 0.1 parts by weight of BaTiSr 0.1 o 3 and conductive carbon mixture with 99.9 parts by weight of LiMnPO 4 Mix, then process at 2500 rpm for 4 minutes, and finally process at 450° C. for 5 hours, so as to prepare a positive electrode active material with a core-shell structure.
[0040] The rest are the same as in Embodiment 1, and will not be repeated here.
Embodiment 3
[0042] Different from Example 1 is the preparation of the positive electrode active material:
[0043] lithium nickel phosphate (LiNiPO 4 , the average particle size is 5000nm) is the active material of the core layer, BaTiPb 0.2 o 3 (average particle size of 100nm) and carbon nanotubes as the shell active material (carbon nanotubes and BaTiPb 0.2 o 3 The mass ratio is 3:97) as the shell active material, and the positive electrode active material with the core-shell structure is prepared. First, 2 parts by weight of BaTiPb were respectively applied using dry coating equipment 0.2 o 3 The mixture with carbon nanotubes was mixed with 98 parts by weight of lithium nickel phosphate, then treated at 2500 rpm for 4 minutes, and finally at 450° C. for 5 hours, so as to prepare a positive electrode active material with a core-shell structure.
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