Active constituent extractor for natural substance
A technology of active ingredients and natural substances, applied in solid solvent extraction, chemical/physical/physical-chemical processes of energy application, etc., can solve problems such as excessive waste of medicinal materials, inability to meet, large differences between production batches, etc., and reduce production costs. , Improve production efficiency and reduce the effect of liquid-material ratio
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Embodiment 1
[0031] Preparation of natural substance active ingredient extractor.
[0032] The natural substance active ingredient extractor, the large liquid tank 4 and the small liquid tank 5 are made of stainless steel with a thickness of 2 mm. The large liquid tank 4 has a volume of 100 liters, and the small liquid tank 5 has a volume of 40 liters. The small liquid tank 5 is set in the large liquid tank 4, and the circulation pump 1 is arranged at the bottom of the large liquid tank 4. The inlet pipe of the circulation pump 1 is connected with the bottom of the large liquid tank 4 ; the outlet of the circulation pump 1 is connected with the upper side wall of the large liquid tank 4 . The large liquid tank 4 is provided with an NTSS2 type temperature sensor 3 . A 15KC type Φ10 ultrasonic horn 6 and a HH-5020-4Z ultrasonic transducer 7 are arranged on the top of the large liquid tank 4 and the small liquid tank 5 . Frame 11 is made of angle steel, and large liquid tank 4 is arranged ...
Embodiment 2
[0033] Embodiment 2: Take the extraction of the active ingredient of Gynostemma pentaphyllum as an example to illustrate the use method of the present invention.
[0034] Taking the extraction of Gynostemma saponins as an example, weigh 2 kg of Gynostemma pentaphyllum dry leaves, grind them into coarse powder for later use. Add the coarse powder of Gynostemma pentaphyllum into the large liquid tank, add pure water according to the ratio of material to liquid 1:35 (g / mL), install the ultrasonic transducer and horn; then turn on the ultrasonic generator and microwave generator in turn, set the ultrasonic The power is 400w, the ultrasonic treatment time is 20min, and the working frequency is 30 times / s; the microwave power is set to 400w, and the extraction temperature is 70°C; the circulation pump is started, and after 50min of dynamic extraction, the liquid outlet switch is turned on to release the extraction liquid. The extract was suction filtered, concentrated and dried to o...
Embodiment 3
[0035] Embodiment 3: Take the extraction of the active ingredient of Chu chrysanthemum as an example to illustrate the method of use of the present invention.
[0036] Taking the extraction of flavonoids from Chu chrysanthemum as an example, weigh 2 kg of dried flowers from Chu chrysanthemum, and crush it into coarse powder for later use. Add chrysanthemum powder into the large liquid tank, add pure water according to the ratio of material to liquid 1:20 (g / mL), install the ultrasonic transducer and horn; then turn on the ultrasonic generator and microwave generator in turn, set the ultrasonic The power is 400w, the working frequency is 30 times / s; the microwave power is set to 400w, and the extraction temperature is 70°C; the circulating pump is started, and after 30 minutes of dynamic extraction, the liquid outlet switch is turned on to release the extraction liquid. The extract was filtered, concentrated and dried to obtain the total flavonoids of chrysanthemum. The extrac...
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