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Active constituent extractor for natural substance

A technology of active ingredients and natural substances, applied in solid solvent extraction, chemical/physical/physical-chemical processes of energy application, etc., can solve problems such as excessive waste of medicinal materials, inability to meet, large differences between production batches, etc., and reduce production costs. , Improve production efficiency and reduce the effect of liquid-material ratio

Inactive Publication Date: 2012-07-18
ANHUI SCI & TECH UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In order to improve the extraction rate of active ingredients, the solvent must be updated at any time to replace the nearly saturated immersion solution, which results in a low output coefficient and large differences between different production batches.
Therefore, the existing equipment cannot further improve the extraction efficiency of the active ingredients of natural substances, which limits the improvement of the quality and use effect of traditional Chinese medicine, food, cosmetics and health care products that rely on the active ingredients of natural substances as raw materials
The disadvantages of the existing equipment are: 1. The extraction rate of active ingredients is low, and there is a lot of waste of medicinal materials; 2. The extraction time is long; 3. The energy consumption of the extraction process is high and the cost is increased; 4. The labor intensity of the operators is high
Since the existing equipment cannot meet the needs of modern industrial production; it cannot meet the needs of raw materials for traditional Chinese medicine, food, cosmetics and health products, so the extraction method of active ingredients of natural substances in the prior art is changed, and a new method with high extraction rate of active ingredients and short extraction time is invented. It is very important to extract the active ingredients of natural substances with low extraction cost

Method used

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  • Active constituent extractor for natural substance
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Preparation of natural substance active ingredient extractor.

[0032] The natural substance active ingredient extractor, the large liquid tank 4 and the small liquid tank 5 are made of stainless steel with a thickness of 2 mm. The large liquid tank 4 has a volume of 100 liters, and the small liquid tank 5 has a volume of 40 liters. The small liquid tank 5 is set in the large liquid tank 4, and the circulation pump 1 is arranged at the bottom of the large liquid tank 4. The inlet pipe of the circulation pump 1 is connected with the bottom of the large liquid tank 4 ; the outlet of the circulation pump 1 is connected with the upper side wall of the large liquid tank 4 . The large liquid tank 4 is provided with an NTSS2 type temperature sensor 3 . A 15KC type Φ10 ultrasonic horn 6 and a HH-5020-4Z ultrasonic transducer 7 are arranged on the top of the large liquid tank 4 and the small liquid tank 5 . Frame 11 is made of angle steel, and large liquid tank 4 is arranged ...

Embodiment 2

[0033] Embodiment 2: Take the extraction of the active ingredient of Gynostemma pentaphyllum as an example to illustrate the use method of the present invention.

[0034] Taking the extraction of Gynostemma saponins as an example, weigh 2 kg of Gynostemma pentaphyllum dry leaves, grind them into coarse powder for later use. Add the coarse powder of Gynostemma pentaphyllum into the large liquid tank, add pure water according to the ratio of material to liquid 1:35 (g / mL), install the ultrasonic transducer and horn; then turn on the ultrasonic generator and microwave generator in turn, set the ultrasonic The power is 400w, the ultrasonic treatment time is 20min, and the working frequency is 30 times / s; the microwave power is set to 400w, and the extraction temperature is 70°C; the circulation pump is started, and after 50min of dynamic extraction, the liquid outlet switch is turned on to release the extraction liquid. The extract was suction filtered, concentrated and dried to o...

Embodiment 3

[0035] Embodiment 3: Take the extraction of the active ingredient of Chu chrysanthemum as an example to illustrate the method of use of the present invention.

[0036] Taking the extraction of flavonoids from Chu chrysanthemum as an example, weigh 2 kg of dried flowers from Chu chrysanthemum, and crush it into coarse powder for later use. Add chrysanthemum powder into the large liquid tank, add pure water according to the ratio of material to liquid 1:20 (g / mL), install the ultrasonic transducer and horn; then turn on the ultrasonic generator and microwave generator in turn, set the ultrasonic The power is 400w, the working frequency is 30 times / s; the microwave power is set to 400w, and the extraction temperature is 70°C; the circulating pump is started, and after 30 minutes of dynamic extraction, the liquid outlet switch is turned on to release the extraction liquid. The extract was filtered, concentrated and dried to obtain the total flavonoids of chrysanthemum. The extrac...

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Abstract

The invention belongs to substance extraction equipment, in particular relates to an active constituent extractor for a natural substance, and aims to solve the defects of low active constituent extraction efficiency, long extraction time and high cost in the prior art. A small liquid box (5) is sleeved in a large liquid box (4); a circulation pump (1) is arranged on the lower part of the large liquid box (4); an inlet of the circulation pump (1) is connected with the bottom of the large liquid box (4); an outlet of the circulation pump (1) is connected with the upper part of the large liquid box (4); a temperature sensor (3) is arranged in the large liquid box (4); an ultrasonic amplitude transformer (6) and an ultrasonic transducer (7) are arranged on the upper parts of the large liquid box (4) and the small liquid box (5); a microwave generator (10) and an ultrasonic generator (9) are arranged on the upper part of a stander (11); and one end of the microwave magnetic tube (8) is connected with the microwave generator (10), and the other end of the microwave magnetic tube (8) is embedded on the side wall of the large liquid box (4). The active constituent extractor for the natural substance has the advantages that: by adopting a circulation liquid flow, microwave and ultrasonic combined extraction technology, the extraction rate is high, and the energy consumption is low.

Description

technical field [0001] The invention belongs to material extraction equipment, in particular to an extractor for effective components of natural substances. Background technique [0002] It is very important to extract active ingredients from natural substances as raw materials for traditional Chinese medicine, food, cosmetics and health care products. Especially for botanical products, it is even more important. In 2006, the global output value of botanical medicine was 35 billion US dollars, and in 2010 it reached 100 billion US dollars. The market demand is very broad. As the birthplace and main place of production of traditional Chinese medicine, China currently produces only 3% of the international market for natural plant medicine products, and in this extremely limited share, most of them are primary raw materials. In the prior art, the equipment and technology for extracting active ingredients of natural substances are backward. The technologies currently used mai...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D11/02B01J19/10B01J19/12
Inventor 易克传曾其良乔印虎李慧张海涛詹学文
Owner ANHUI SCI & TECH UNIV
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