Toner, image forming method, and process cartridge
A toner and colorant technology, applied in the field of electrophotographic toner, can solve the problems of poor fluorescent color reproducibility, fluorescent colorant reflectivity and poor brightness, etc.
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[0103] Preparation of polyester resin A1~A6
[0104] A 5 liter autoclave equipped with a distillation column was charged with 4,000 g of alcohol and carboxylic acid monomers according to the composition stated in Table 1 . In the absence of a catalyst, the monomer is subjected to an esterification reaction at 170-260° C. under normal pressure. After further adding antimony trioxide in an amount of 400 ppm based on the total weight of the carboxylic acid monomers, the monomers were subjected to polycondensation under a vacuum of 3 Torr at 250° C. while removing generated diols. Thus, polyester resins A1 to A6 were prepared. The crosslinking reaction was continued until the stirring torque became 10 kg·cm (100 ppm). The reaction was stopped by releasing the reduced pressure conditions.
[0105] Table 1
[0106]
[0107] * BPA-PO: Polyoxypropylene (2,2)-2,2-bis(4-hydroxyphenyl)propane
[0108] ** BPA-EO: Polyoxyethylene (2,2)-2,2-bis(4-hydroxyphenyl)propane
[0109] Ev...
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