Composite bactericide containing solidago canadensis extract
A technology of compound fungicides and extracts, applied in the directions of fungicides, biocides, biocides, etc., can solve the problem of low activity of fungicides, reduce the use, be beneficial to pollution-free agricultural production, and effectively kill insects and prevent effect of effect
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Embodiment 1
[0034] Embodiment 1: Preparation of Solidago canadensis Extract
[0035] Clean the fresh Solidago canadensis, dry and crush it to obtain powder, weigh 10kg of powder and soak it in 20kg of anhydrous methanol for 12h at 25~30℃, filter, take the filter cake and add 20kg of anhydrous methanol to extract under the same conditions 8h, filter again, take the filter cake filtered again and add 20kg of anhydrous methanol to leach for 8h under the same conditions, filter three times, combine all the filtrates obtained by three extractions, filter, concentrate under vacuum and reduce pressure until no solvent flows out, that is, methanol is removed (Methanol is recovered and recycled), the concentrate is obtained, and the concentrate is taken to prepare 500 grams of Solidago canadensis extract.
Embodiment 2
[0036] Example 2: Compound effect of Solidago canadensis extract and several chemical fungicides
[0037] The solidago canadensis extract prepared by the method in Example 1 was mixed with fungicides (carbendazim, thiophanate-methyl, flusilazole or chlorothalonil) according to the mass ratio shown in Table 1 to test the co-toxicity coefficient. See: (South China Agricultural University. Phytochemical Protection [M] 2nd Edition [M]. Beijing: Agricultural Publishing House, 1990), the results are shown in Table 1.
[0038] Table 1 Synergistic effect of Solidago canadensis extract and several pesticides
[0039]
[0040]
[0041] *Note: The co-toxicity coefficient is greater than 100, indicating that the combination of the two has a synergistic effect.
Embodiment 3
[0042] Example 3: Composite fungicide (product one)
[0043] 10 grams of Solidago canadensis extract prepared by the method of Example 1, 20 grams of carbendazim, 5 grams of sodium lignosulfonate, 2 grams of dispersant NNO, 0.5 grams of sodium lauryl sulfate, light calcium carbonate supplemented to 100 grams, the above-mentioned samples were thoroughly mixed and then jet-milled to make (pesticide) wettable powder with a mass concentration of 30%, that is, compound fungicide wettable powder.
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