Manufacturing method and application of PDMS (Polydimethylsiloxane) polymer chip with arc sunk holes
A polymer and polymer solution technology, applied in biochemical equipment and methods, combinatorial chemistry, library creation, etc., can solve the problems of high price and complicated operation, and achieve the effect of simple operation and low experimental cost
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Embodiment 1
[0034] The PDMS channel template is made by soft etching technology, the template is a 12×12 circular hole, and the template structure is cylindrical. Prepare an uncured PDMS (10:1) solution, pour a certain amount of PDMS solution on a clean silicon wafer at a speed of 5,000 rpm, uniform the glue on a homogenizer for one minute, and then heat and cure at 80°C for 2 hours. Using plasma technology to seal PDMS templates and thin films, glass sheets, forming such as figure 1 installation. After the whole device was silanized for 5 minutes, connect the air cylinder, control the amount of gas entering by adjusting the air pressure, pour the uncured PDMS (10:1), feed the gas, and heat at 80°C for 20 minutes at the same time. After the device is cooled, a PDMS chip is placed on the glass to form an arc-shaped PDMS polymer chip with concave holes.
Embodiment 2
[0036] The principle and flow chart of the three-dimensional cell culture on the PDMS polymer chip with arc-shaped concave holes are as follows figure 2 shown. The PDMS polymer chip with arc-shaped concave holes is first sterilized, irradiated with ultraviolet light overnight, and then modified with 1% PF-127 solution for 8 hours, inoculated with cell suspension, and the cells will precipitate under the action of gravity To the bottom of the small wells on the surface of the chip, three-dimensional cell clusters are spontaneously formed.
Embodiment 3
[0038] Characterization of the height of a PDMS polymer chip based on pneumatically fabricated arcuate recessed apertures. image 3 The height of the arc-shaped concave holes on the surface of the PDMS polymer chip is shown under different gas pressure conditions. and image 3 A in a shows the height difference of the small holes on the surface of the PDMS polymer chip under the same air pressure conditions at different positions, which shows that arc-shaped concave small holes of different heights can be simultaneously produced under the same control conditions by this method. image 3The c in the figure shows that different heights of small holes can be formed under different air pressure conditions, which shows that arc-shaped concave small holes with different heights can be significantly controlled by this method.
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