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High concentration sericite master batch and preparation method and application thereof

A sericite, high-concentration technology, applied in the direction of mechanical equipment, rigid pipes, pipes/pipe joints/pipe fittings, etc., can solve problems such as unsatisfactory results, shorten the processing route, save energy, and improve heat resistance. Effect

Active Publication Date: 2012-12-05
江苏祥华科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the large amount of free water adsorbed on the surface of sericite powder, the effect of surface treatment with coupling agent is not ideal

Method used

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  • High concentration sericite master batch and preparation method and application thereof
  • High concentration sericite master batch and preparation method and application thereof
  • High concentration sericite master batch and preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Material:

[0033] (1) The mass ratio of each component in the high-concentration sericite material is: sericite powder (wet process sericite powder, particle size 200 mesh, produced by Anhui Chuzhou Wenlong Sericite Co., Ltd., the same below) 80 parts; resin Acid (first grade, Guangxi Xing'an County Rosin Factory, the same below) 1 part, wherein the resin acid is resin acid extracted from rosin, which is C 19 h 29 A mixture of organic carboxylic acids of isomers of COOH; the dispersant is 5 parts of oxidized PE wax dispersant (PEWO-0503, produced by Nanjing Tianshi Micro Powder Co., Ltd., the same below); antioxidant 1010 (Jinhai Yabao Co., Ltd. Production, the same below) 0.01 parts; recycled HDPE (milk bottle crushed recycled materials, provided by Jiangsu Shengtong Environmental Engineering Company, the same below) 20 parts.

[0034] The preparation method of high concentration sericite material:

[0035] Add sericite powder into the high-speed mixer and raise th...

Embodiment 2

[0041] Material:

[0042] (1) The mass ratio of each component in the high-concentration sericite material is: 150 parts of sericite powder, 10 parts of resin acid, 20 parts of oxidized PE wax, 0.1 part of antioxidant 1010, and 30 parts of recycled HDPE, of which Resin acid is resin acid extracted from rosin, which is C 19 h 29 A mixture of organic carboxylic acids that are isomers of COOH. High concentration sericite material preparation method is the same as embodiment 1

[0043] (2) The mass ratio of each component of the hollow winding pipe is: 15 parts of high-concentration sericite material, 100 parts of recycled HDPE, and 0.2 part of black mother.

[0044] Preparation method of hollow wound pipe: same as in Example 1.

[0045] For the hollow wound pipe prepared in Example 2, performance tests such as ring stiffness were carried out according to GB / T14152-2004. Test results: see Table 1.

Embodiment 3

[0047] Material:

[0048] (1) The mass ratio of each component in the high-concentration sericite material is: 120 parts of sericite powder, 7 parts of resin acid, zinc stearate (industrial grade, produced by Jiangsu Nantong Huizhi Chemical Co., Ltd., the same below) 15 parts, 0.06 parts of antioxidant 1010, and 30 parts of recovered HDPE.

[0049] (2) The mass ratio of each component of the hollow pipe is: 20 parts of high-concentration sericite material, 100 parts of recycled HDPE, and 0.5 part of black mother.

[0050] The preparation method of high-concentration sericite material: the same as Example 1, the difference is that after adding sericite powder in the high-speed mixer, the temperature is raised to 108 ° C, and after preheating for 15 minutes, resin acid and antioxidant 1010 are added and stirred at high speed Mix for 8 minutes, then add zinc stearate and recovered HDPE, stir for about 20 minutes, and discharge.

[0051] Preparation method of hollow wound pipe: ...

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Abstract

The invention discloses a method for preparing high concentration sericite master batch and an application thereof. The high concentration sericite master batch includes 80-150 portions of sericite powder, 1-10 portions of resin acid, 5-20 portions of dispersant, 0.1-0.01 portions of antioxidant 1010 and 10-30 portions of recycled HDPE (high-density polyethylene). Sericite power is added to the high-speed mixer and heated to 105-110 DEG C. After 10 minutes of preheating, resin acid and antioxidant 1010 are added and mixed in high speed for 5-10 minutes. Then the oxidized PE wax and recycled HDPE are added. 10-30 minutes of mixing is needed before discharging. Mixture is fed in the twin-screw extruder for prilling to obtain sericite master batch and then produce the hollow winding pipe. The method significantly improves the rigidity of the recycled HDPE and also improves the ring rigidity of the prepared hollow winding pipe. Meanwhile, the prepared sericite master batch can be mixed with the recycled HDPE conveniently to produce the hollow winding pipe directly, thereby saving both production cost and energy.

Description

technical field [0001] The invention relates to a master material of sericite powder with reinforcing effect, in particular to a high-concentration sericite material and its preparation and application, which utilizes the flaky anisotropic characteristics of mica to strengthen and recycle HDPE to produce low-cost and high-strength Large-diameter hollow winding pipes are used for urban drainage. Background technique [0002] Plastic products have been widely used in all fields including industrial and agricultural production, construction, municipal construction, national defense construction, transportation, energy transmission, packaging industry, daily life, etc., and our country has discarded more than 3 million tons of plastic every year. Degradation in a short period of time has caused great pressure on my country's ecological environment. Recycling and reusing waste plastics has huge economic and social benefits. The development of the waste plastics recycling industry...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08K3/34C08K5/09C08K5/134C08L23/06C08J3/22B29C47/92F16L9/12B29C48/92
CPCB29C48/04B29C48/40B29C48/875B29C48/92B29C2948/92704B29C2948/92895B29C2948/92904
Inventor 陈正年黄玉安肖浪刘兆亮陶祝庆王强
Owner 江苏祥华科技有限公司
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