Preparation method of foaming agent for use in burning of refractory brick
A technology of foaming agent and refractory brick, which is applied in the field of foaming agent preparation, can solve the problems affecting the thermal insulation performance of refractory bricks, the difference in pore size of refractory bricks, and the uneven density of refractory bricks, so as to reduce the gas permeability and internal pores. Meticulous and uniform, reducing the effect of caustic soda residue
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Embodiment 1
[0012] (1) Water and caustic soda are mixed with 1000ml water and 300ml caustic soda according to the volume ratio of 1:0.3 and heated to 70°C with water, and the required rosin weight is calculated as 350g according to the water-to-rosin weight ratio of 1:0.35, and the required weight Grind the rosin into particles with a diameter of ≤5mm and put it into the caustic soda solution to continue heating with water to boil it into a milky white block rosin soap;
[0013] (2) After the rosin soap obtained in step (1) is cooled, it is put into concentrated brine with a concentration of 15% and soaked for 2 hours, then taken out and rinsed with clear water until the pH value is 9;
[0014] (3) Mix water and bone glue in a weight ratio of 1:0.25 and heat to form a bone glue solution, mix the bone glue solution with the rosin soap after rinsing in step (2) in a weight ratio of 1:0.15, and heat until the rosin soap is completely dissolved to obtain burnt Foaming agent for refractory bri...
Embodiment 2
[0016] (1) Water and caustic soda are mixed with 1000ml water and 350ml caustic soda according to the volume ratio of 1:0.35 and heated to 80°C in water, and the weight of rosin required for calculating the weight ratio of water to rosin is 1:0.45 is 450g, and the required weight Grind the rosin into particles with a diameter of ≤5mm and put it into the caustic soda solution to continue heating with water to boil it into a milky white block rosin soap;
[0017] (2) After the rosin soap obtained in step (1) is cooled, it is put into concentrated brine with a concentration of 16% and soaked for 3 hours, then taken out and rinsed with clear water until the pH value is 8;
[0018] (3) Mix water and bone glue in a weight ratio of 1:0.27 and heat to form a bone glue solution, mix the bone glue solution with the rosin soap after rinsing in step (2) in a weight ratio of 1:0.18, and heat until the rosin soap is completely dissolved to obtain burnt Foaming agent for refractory bricks. ...
Embodiment 3
[0020] (1) Water and caustic soda are mixed with 1000ml water and 430ml caustic soda according to the volume ratio of 1:0.43 and heated to 75°C in water, and the required rosin weight is calculated according to the weight ratio of water and rosin of 1:0.5 to be 500g, and the required weight Grind the rosin into particles with a diameter of ≤5mm and put it into the caustic soda solution to continue heating with water to boil it into a milky white block rosin soap;
[0021] (2) After the rosin soap obtained in step (1) is cooled, put it into concentrated brine with a concentration of 17% and soak for 2.5 hours, then take it out and rinse it with clear water until the pH value is 8.7;
[0022] (3) Mix water and bone glue in a weight ratio of 1:0.35 and heat to form a bone glue solution, mix the bone glue solution with the rosin soap after rinsing in step (2) in a weight ratio of 1:0.2, and heat until the rosin soap is completely dissolved. Foaming agent for refractory bricks.
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