Liquid filtration method
A filtration method and liquid technology, which can be applied in filtration separation, membrane filter, liquid degassing and other directions, can solve the problem that the filter cannot obtain sufficient effect, and achieve the effect of improving filtration efficiency, low cost, and long life.
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Embodiment 1~6
[0048] As a filter member for filtering non-degassed liquid, prepare a depth filter with a total length of about 50 cm (filter size: total length about 50 cm; outer diameter about 7 cm; inner diameter about 2.8 cm), and follow the pretreatment conditions shown below Deaerated water was passed through it, and pretreatment was carried out.
[0049] pretreatment conditions
[0050] Degassed water flow rate: 19L / min
[0051] Degassed water flow time: 0.25 minutes, 0.5 minutes, 1 minute, 2 minutes, 5 minutes or 30 minutes
[0052] Dissolved oxygen concentration in degassed water: 0.5mg / L
[0053] Degassed water production method: Membrane degassing method (a method in which ultrapure water is introduced into the hollow fiber membrane module to make the outside of it a vacuum, thereby removing the dissolved gas (hollow fiber: poly-4-methylpentane ene-1, vacuum pressure: 2.7kPa))
[0054] Next, non-degassed ultrapure water was prepared as the non-degassed liquid, and the filtrati...
Embodiment 7 and comparative example 7
[0068] A filter having the same material and shape as in Example 1 was prepared except for the filtration precision, and pretreated under the following conditions.
[0069] Degassed water flow rate: 15L / min
[0070] Degassed water flow time: 3.3 minutes
[0071] The volume ratio X / Y of the throughput X of the degassing liquid to the capacity Y of the filter member:
[0072] 40
[0073] Dissolved oxygen concentration in degassed water and degassed water manufacturing method: same as Example 1
[0074] Next, as the non-degassed liquid to be filtered, a polishing slurry containing fumed silica having an average particle diameter of 30 nm at a concentration of 13% by weight was prepared, and filtered using a pretreated filter according to the following procedure: condition to filter. At this time, the filtration efficiency was measured immediately after the start of filtration, when 100 L was passed, when 200 L was passed, and when 300 L was passed. In addition, the time requ...
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