Method for detecting milk adulteration

A technology of detection method and measurement method, which is applied in the direction of testing food, dairy products, material inspection products, etc., and can solve problems such as advanced adulteration

Active Publication Date: 2015-01-07
BRIGHT DAIRY & FOOD CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although these methods can judge the quality of milk to a certain extent, it is difficult to take into account both the technical personnel's requirements for equipment and instrument operation and the targeted high-level adulteration at the same time, which has certain limitations.

Method used

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  • Method for detecting milk adulteration
  • Method for detecting milk adulteration

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1-20

[0029] Different raw milk samples and adulterated cow milk added with different adulterants are selected, and adulteration detection is performed according to the method of the present invention. The specific components are shown in Table 1 below:

[0030] Table 1 Sample composition of Examples 1-20

[0031] Example

Type of sample (adultant)

Water content

Adulteration

1

Normal milk

0

0

2

Normal milk

0

0

3

Normal milk

0

0

4

Normal milk

0

0

5

Normal milk

0

0

6

Normal milk

0

0

7

Normal milk

0

0

8

Normal milk

0

0

9

Normal milk

0

0

10

Normal milk

0

0

11

Adulterated milk (reduced fat 50% milk + butter)

0

50%

12

Adulterated milk (non-dairy fat)

5%

5%

13

Adulterated milk (ammonium salt)

5%

10%

14

Adulterated milk (urea)

5%

5%

15

Adulterated milk (gelatin protein)

5%

7%

16

Adulterated milk (melamine)

5%

7%

17

Adulterated milk (non-dairy fat + melamine + d...

Embodiment 21

[0045] For raw milk, the total solids, fat, lactose content, and freezing point determined by the method in Example 1 were 12.79g / 100g milk, 3.62g / 100g milk, 4.99g / 100g milk and -0.533°C, respectively. The calculated Q factor is 0.000411, which is judged to be normal according to the evaluation system. The sample is raw milk for production that meets the standard. The evaluation result is consistent with the actual sample.

Embodiment 22

[0047] Raw milk (adulterated with water, non-dairy fat, ammonium salt, dextrin, the amount of water is 5%, and the amount of non-dairy fat, ammonium salt, and dextrin is 7% each, the unit is the same as in Example 1), according to the implementation The method of Example 1 measured total solids, fat, lactose content and freezing point as 10.9g / 100g milk, 3.11g / 100g milk, 4.96g / 100g milk and -0.609°C, respectively. The calculated Q factor is -0.01779. According to the evaluation system, it is judged to be adulterated. This sample is adulterated raw milk with whey added. The evaluation result is consistent with the actual sample.

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Abstract

The invention discloses a method for detecting milk adulteration. The method comprises the following steps: (1) respectively measuring total milk solid based on g / 100g of milk, fat based on g / 100g of milk, an ice point based on DEG C, and milk sugar based on g / 100g of milk, and orderly marking numerical values to be ST, Fat, FPD and La; (2) substituting the total solid content of the milk, the fat content, the ice point and the milk sugar content into the following formula to calculate a characteristic index coefficient Q, Q=(1.486Fat-ST+7.229)*(-0.074Lac-FPD-0.166); (3) judging whether the milk is adulterated or not according to the milk characteristic index coefficient Q, and judging the milk to be normal when the numerical value of Q meets the condition that Q is smaller than or equal to 0.0036 and greater than or equal to -0.0036, and judging the milk to be adulterated milk when the numerical value of Q is smaller than -0.0036 or greater than 0.0036. The method for measuring the milk sugar content is a milk sugar measuring method in import and export milk and milk products. The colorimetric blank dilution ratio of the measured milk is 20-25 fold. The method is comprehensive, effective and fast.

Description

Technical field [0001] The invention belongs to the field of milk quality evaluation, and specifically relates to a detection method of milk adulteration. Background technique [0002] In recent years, my country’s dairy industry has developed rapidly and its product structure has undergone great changes. It has become a modern food manufacturing industry with advanced technology and equipment, a relatively complete range of products, and a beginning to take shape. With the gradual improvement of people’s living standards, the dairy product consumer market will With continuous expansion and maturity, China will become the world's largest potential market for dairy products consumption. However, many problems and hidden dangers have also arisen during the development of the dairy industry, and the safety problems caused by adulteration of dairy products are endless. [0003] In recent years, the research on the detection of adulteration of dairy products has continuously made new pr...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N33/04G01N21/31
Inventor 任婧刘景
Owner BRIGHT DAIRY & FOOD CO LTD
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